Synthesis/characterization of molecular imprinted polymer based on magnetic chitosan/graphene oxide for selective separation/preconcentration of fluoxetine from environmental and biological samples

被引：61

作者：

Barati, Asma ^{[1
]}

Kazemi, Elahe ^{[1
]}

Dadfarnia, Shayessteh ^{[1
]}

Shabani, Ali Mohammad Haji ^{[1
]}

机构：

[1] Yazd Univ, Dept Chem, Safaieh 89195741, Yazd, Iran

来源：

JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY | 2017年 / 46卷

关键词：

Magnetic solid phase extraction; Molecular imprinted polymer; Graphene oxide; Chitosan; Fiber optic linear array spectrophotometry; Fluoxetine; SOLID-PHASE MICROEXTRACTION; PERFORMANCE LIQUID-CHROMATOGRAPHY; GRAPHENE OXIDE; PHARMACEUTICAL FORMULATIONS; MASS-SPECTROMETRY; COMPOSITE FILM; TRACE ANALYSIS; EXTRACTION; CHITOSAN; WATER;

D O I：

10.1016/j.jiec.2016.10.033

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A novel molecular imprinted polymer (MIP) as a SPE sorbent was synthesized for fluoxetine through a coprecipitation method. The synthesized polymer was characterized by Fourier transform infrared (FT-IR) spectroscopy and scanning electron microscopy (SEM). The kinetic and adsorption equilibrium was studied. Quantification of fluoxetine was done based on the competitive inclusion complex formation of fluoxetine with phenolphthalein-p-cyclodextrin using fiber optic linear array spectrophotometry. The method exhibited a linear dynamic range of 0.8-10.0 mu g L-1 with a detection limit of 0.03 mu g L-1 and a preconcentration factor of 500. The developed method was successfully applied to determine fluoxetine in various samples. (C) 2016 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.

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收藏

页码：212 / 221

页数：10

相关论文

共 51 条

[1] Spectrophotometric determination of fluoxetine by batch and flow injection methods [J].

Afkhami, Abbas ;

Madrakian, Tayyebeh ;

Khalafi, Lida .

CHEMICAL & PHARMACEUTICAL BULLETIN, 2006, 54 (12) :1642-1646

[2] Sorption potential of rice husk for the removal of 2,4-dichlorophenol from aqueous solutions: Kinetic and thermodynamic investigations [J].

Akhtar, M ;

Bhanger, MI ;

Iqbal, S ;

Hasany, SM .

JOURNAL OF HAZARDOUS MATERIALS, 2006, 128 (01) :44-52

[3] Arrays of SnO2 nanorods as novel solid phase microextraction for trace analysis of antidepressant drugs in body fluids [J].

Alizadeh, Reza ;

Najafi, Nahid Mashkouri ;

Poursani, Ensieh Mohammad Ali .

JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2012, 70 :492-498

[4] In vitro study on fluoxetine adsorption onto charcoal using potentiometry [J].

Atta-Politou, J ;

Skopelitis, I ;

Apatsidis, I ;

Koupparis, M .

EUROPEAN JOURNAL OF PHARMACEUTICAL SCIENCES, 2001, 12 (03) :311-319

[5] Extraction of fluoxetine from aquatic and urine samples using sodium dodecyl sulfate-coated iron oxide magnetic nanoparticles followed by spectrofluorimetric determination [J].

Bagheri, Habib ;

Zandi, Omid ;

Aghakhani, Ali .

ANALYTICA CHIMICA ACTA, 2011, 692 (1-2) :80-84

[6] Trace analysis of fluoxetine and its metabolite norfluoxetine. Part II: Enantioselective quantification and studies of matrix effects in raw and treated wastewater by solid phase extraction and liquid chromatography-tandem mass spectrometry [J].

Barclay, Victoria K. H. ;

Tyrefors, Niklas L. ;

Johansson, I. Monika ;

Pettersson, Curt E. .

JOURNAL OF CHROMATOGRAPHY A, 2012, 1227 :105-114

[7] FLUOXETINE - A REVIEW OF ITS PHARMACODYNAMIC AND PHARMACOKINETIC PROPERTIES, AND THERAPEUTIC EFFICACY IN DEPRESSIVE-ILLNESS [J].

BENFIELD, P ;

HEEL, RC ;

LEWIS, SP .

DRUGS, 1986, 32 (06) :481-508

[8] Sensitive spectrophotometric determination of fluoxetine from urine samples using charge transfer complex formation after solid phase extraction by magnetic multiwalled carbon nanotubes [J].

Bigdelifam, Davood ;

Mirzaei, Mohammad ;

Hashemi, Mahdi ;

Amoli-Diva, Mitra ;

Rahmani, Omid ;

Zohrabi, Parvin ;

Taherimaslak, Zohreh ;

Turkjokar, Mohammad .

ANALYTICAL METHODS, 2014, 6 (21) :8633-8639

[9] Adsorption of congo red by chitosan hydrogel beads impregnated with carbon nanotubes [J].

Chatterjee, Sudipta ;

Lee, Min W. ;

Woo, Seung H. .

BIORESOURCE TECHNOLOGY, 2010, 101 (06) :1800-1806

[10] The development of a new disposable pipette extraction phase based on polyaniline composites for the determination of levels of antidepressants in plasma samples [J].

Chaves, Andrea R. ;

Moura, Bruno H. F. ;

Caris, Juciene A. ;

Rabelo, Denilson ;

Queiroz, Maria Eugenia C. .

JOURNAL OF CHROMATOGRAPHY A, 2015, 1399 :1-7

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