3D grain reconstruction from laboratory diffraction contrast tomography

被引:57
作者
Bachmann, Florian [1 ]
Bale, Hrishikesh [2 ]
Gueninchault, Nicolas [1 ]
Holzner, Christian [1 ,2 ]
Lauridsen, Erik Mejdal [1 ]
机构
[1] Xnovo Technol ApS, Theilgaards Alle 9,1th, DK-4600 Kooge, Denmark
[2] Carl Zeiss Xray Microscopy, 4385 Hopyard Rd, Pleasanton, CA 94588 USA
关键词
three-dimensional X-ray diffraction (3DXRD); grain mapping; DCT; X-ray diffraction contrast microscopy; reconstruction schemes; X-RAY-DIFFRACTION; ORIENTATION; POLYCRYSTALS; STRAIN; MICROSCOPY; GROWTH; STATE; MAPS;
D O I
10.1107/S1600576719005442
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A method for reconstructing the three-dimensional grain structure from data collected with a recently introduced laboratory-based X-ray diffraction contrast tomography system is presented. Diffraction contrast patterns are recorded in Laue-focusing geometry. The diffraction geometry exposes shape information within recorded diffraction spots. In order to yield the three-dimensional crystallographic microstructure, diffraction spots are extracted and fed into a reconstruction scheme. The scheme successively traverses and refines solution space until a reasonable reconstruction is reached. This unique reconstruction approach produces results efficiently and fast for well suited samples.
引用
收藏
页码:643 / 651
页数:9
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