Growth of Y1-zNdzBa2Cu3Ox single crystals

被引:6
作者
Aswal, DK [1 ]
Mori, T [1 ]
Hayakawa, Y [1 ]
Kumagawa, M [1 ]
机构
[1] Shizuoka Univ, Elect Res Inst, Hamamatsu, Shizuoka 4328011, Japan
基金
日本学术振兴会;
关键词
flux-growth; phase diagram; high-temperature optical microscopy; Y0.5Nd0.5Ba2Cu3Ox;
D O I
10.1016/S0022-0248(99)00391-7
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The growth of Y1-zNdzBa2Cu3Ox single crystals has been carried out using self-flux Ba3Cu10O13 in alumina crucibles under a horizontal temperature gradient. The optimum growth conditions such as solute-to-flux ratio, maximum growth temperature, cooling rate, etc. were obtained by investigating the pseudo-binary Y0.5Nd0.5Ba2Cu3Ox-Ba3Cu10O13 phase diagram and crystallization mechanism of Y0.5Nd0.5Ba2Cu3Ox using in situ high-temperature optical microscopy. Plate-like Y1-zNdzBa2Cu3Ox crystals up to a size of 7.3 x 5.8 x 1.28 mm(3) exhibiting superconductivity at 93 K have been grown. The crystallinity of the grown crystals has been confirmed by Laue X-ray backscattering measurements. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:350 / 356
页数:7
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