Experimental Investigations in Liquid-Liquid Dispersion System: Effects of Dispersed Phase Viscosity and Impeller Speed

被引:17
作者
Abidin, Mohd Izzudin Izzat Zainal [1 ]
Raman, Abdul Aziz Abdul [1 ]
Nor, Mohamad Iskandr Mohamad [1 ]
机构
[1] Univ Malaya, Fac Engn, Dept Chem Engn, Kuala Lumpur 50603, Malaysia
关键词
DROP SIZE DISTRIBUTION; STIRRED-TANK CONTACTORS; TURBULENT DISPERSIONS; AGITATED VESSELS; SUSPENSION POLYMERIZATION; WATER DISPERSION; OIL FRACTIONS; SCALE-UP; DISTRIBUTIONS; BREAKUP;
D O I
10.1021/ie5002845
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Experimental investigation was conducted on a liquid-liquid dispersion in a stirred vessel in which the effects of dispersed phase viscosity were studied. Different grades of silicone oils were used to create oil-in-water dispersion by using Rushton turbine as an impeller, and drop sizes were measured by laser diffraction technique. Dispersion with higher uniformity of drop sizes was produced at low viscosity and high impeller speed. The dispersed phase viscosity influenced the equilibrium Sauter mean diameter, d(32) by contributing to drops stabilization. The decrement of d(32) with an increase in impeller speed is larger for high dispersed phase viscosities. It shows the influence of number and size of drop fragments formed after drop breakup on the mean drop size. Correlations relating d(32) and dispersed phase viscosity were proposed with an accuracy of more than 90% between the predicted and experimental values.
引用
收藏
页码:6554 / 6561
页数:8
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