THE SYNTHESIS OF DIPYRAZOLYLMETHANES, X-RAY STRUCTURE ANALYSIS

被引:1
作者
Ma, Yuan [1 ]
Wang, Jinxia [1 ]
Ma, Hengchang [1 ]
机构
[1] Northwest Normal Univ, Coll Chem & Chem Engn, Key Lab Polymer Mat Gansu Prov, Key Lab Ecoenvironm Related Polymer Mat,Minist Ed, Lanzhou 730070, Peoples R China
基金
中国国家自然科学基金;
关键词
RUBAZOIC ACID-DERIVATIVES; 4-(5-HYDROXY-4-PYRAZOLYLIMINO)-2-PYRAZOLIN-5-ONES; TRANSFORMATIONS; NUCLEOPHILES; CARBONYLS; OXIDATION; ALCOHOLS; INDOLES;
D O I
10.3987/COM-13-12840
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A small dipyrazoylmethane compounds library was established via the reaction of 5-alkyl- and 5-aryl-2-aryl-3H-pyrazol-3-ones with DMSO in the presence of NaOAc center dot 3H(2)O as base using LiBr center dot H2O as additive at 100 degrees C.
引用
收藏
页码:1645 / 1655
页数:11
相关论文
共 21 条
  • [1] [Anonymous], ADV MOL STRUCT RES
  • [2] [Anonymous], 850167 CCDC
  • [3] AZEV YA, 1995, MENDELEEV COMMUN, P229
  • [4] Peculiarities of transformations of unsubstituted quinazoline with C-nucleophiles
    Azev, Yu. A.
    Shorshnev, S. V.
    [J]. CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2009, 45 (01) : 115 - 116
  • [5] Specific features of the reactions of quinazoline and its 4-hydroxy and 4-chloro substituted derivatives with C-nucleophiles
    Azev, Yuri A.
    Shorshnev, Sergey V.
    Golomolzin, Boris V.
    [J]. TETRAHEDRON LETTERS, 2009, 50 (24) : 2899 - 2903
  • [6] Reactions of quinoxaline with 3-methyl-1-phenylpyrazol-5-one
    Azev, Yurii A.
    Oparina, Elena D.
    Kovalev, Igor S.
    Slepukhin, Pavel A.
    Novikova, Rashida K.
    [J]. MENDELEEV COMMUNICATIONS, 2012, 22 (01) : 37 - 38
  • [7] Synthesis and crystal structure of 2,4-dihydro-4-[(5-hydroxy-3methyl-1-phenyl-1H-pyrazol-4-yl)imino]-5-methyl-2-phenyl-3H-pyrazol-3-one and its copper(II) complex
    Cerchiaro, Giselle
    Da Costa Ferreira, Ana M.
    Teixeira, Aline B.
    Magalhaes, Hugo M.
    Cunha, Anna C.
    Ferreira, Vitor F.
    Santos, Leonardo S.
    Eberlin, Marcos N.
    Skakle, Janet M. S.
    Wardell, Solange M. S. V.
    Wardell, James L.
    [J]. POLYHEDRON, 2006, 25 (10) : 2055 - 2064
  • [8] THE STRUCTURES OF 2 RUBAZOIC ACID-DERIVATIVES
    DRUCK, U
    LITTKE, W
    [J]. ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1980, 36 (DEC): : 3002 - 3007
  • [9] The ammonium-promoted formylation of indoles by DMSO and H2O
    Fei, Haiyang
    Yu, Jintao
    Jiang, Yan
    Guo, Huan
    Cheng, Jiang
    [J]. ORGANIC & BIOMOLECULAR CHEMISTRY, 2013, 11 (41) : 7092 - 7095
  • [10] HANSEL W, 1976, LIEBIGS ANN CHEM, P1380