Stress analysis of zirconia studied by Raman spectroscopy at low temperatures

被引：11
作者：
Kurpaska, L. [1 ]
Kozanecki, M. [2 ]
Jasinski, J. J. [3 ]
Sitarz, M. [4 ]
机构：
[1] Natl Ctr Nucl Res, PL-05400 Otwock, Poland
[2] Lodz Univ Technol, Fac Chem, Dept Mol Phys, PL-90924 Lodz, Poland
[3] Czestochowa Tech Univ, Inst Mat Sci, PL-42200 Czestochowa, Poland
[4] AGH Univ Sci & Technol, Fac Mat Sci & Ceram, PL-30059 Krakow, Poland
来源：
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2014年 / 131卷
关键词：
Oxide scale stress; Raman spectroscopy; Low temperature studies; OXIDE-FILMS; EVOLUTION; ZRO2; XRD;
D O I：
10.1016/j.saa.2014.05.023
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
The paper presents effect of low temperature upon location of selected Raman bands. The structural properties of pure zirconium pre-oxidized at 773 K and 873 K have been studied during cooling in the range of temperatures 273 K and 93 K by Raman spectroscopy. Analysis of the Raman band positions for the monoclinic phase of zirconia oxide was performed. Raman spectroscopy has shown that monoclinic phase of zirconia oxide undergoes a continuous band displacement, individual for each studied Raman mode. Registered shift is aimed towards the high frequency direction. Recorded Raman band displacement was employed to study stress state in zirconia oxide films grown on pure zirconium developed during control cooling. Presented results showed a good correlation between different thicknesses of the oxide scale. (C) 2014 Elsevier B.V. All rights reserved.
引用
收藏
页码：691 / 695
页数：5
相关论文
共 16 条
  • [1] On Raman spectroscopy of zirconium oxide films
    Barberis, P
    MerleMejean, T
    Quintard, P
    [J]. JOURNAL OF NUCLEAR MATERIALS, 1997, 246 (2-3) : 232 - 243
  • [2] ZIRCONIA POWDERS AND ZIRCALOY OXIDE-FILMS - TETRAGONAL PHASE EVOLUTION DURING 400-DEGREES-C AUTOCLAVE TESTS
    BARBERIS, P
    [J]. JOURNAL OF NUCLEAR MATERIALS, 1995, 226 (1-2) : 34 - 43
  • [3] Raman spectra and vibrational analysis of nanometric tetragonal zirconia under high pressure
    Bouvier, P
    Lucazeau, G
    [J]. JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2000, 61 (04) : 569 - 578
  • [4] Low temperature phase transformation of nanocrystalline tetragonal ZrO2 by neutrons and Raman Scattering studies
    Bouvier, P
    Djurado, E
    Ritter, C
    Dianoux, AJ
    Lucazeau, G
    [J]. INTERNATIONAL JOURNAL OF INORGANIC MATERIALS, 2001, 3 (07): : 647 - 654
  • [5] Bouvier P., 2000, THESIS I NATL POLITE
  • [6] Crystallite size effect on the tetragonal-monoclinic transition of undoped nanocrystalline zirconia studied by XRD and Raman spectrometry
    Djurado, E
    Bouvier, P
    Lucazeau, G
    [J]. JOURNAL OF SOLID STATE CHEMISTRY, 2000, 149 (02) : 399 - 407
  • [7] Godlewski J., 1990, THESIS UTC COMPIEGNE
  • [8] Godlewski J., 1994, 10 INT S ZIRC NUCL I
  • [9] Modelling of stresses evolution in growing thermal oxides on metals. A methodology to identify the corresponding mechanical parameters
    Grosseau-Poussard, J. -L.
    Panicaud, B.
    Ben Afia, S.
    [J]. COMPUTATIONAL MATERIALS SCIENCE, 2013, 71 : 47 - 55
  • [10] Kurpaska L., 2013, OXID MET UNPUB
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