The synthesis of a novel graphene-based inorganic-organic hybrid flame retardant and its application in epoxy resin

被引:159
作者
Wang, Zehao [1 ]
Wei, Ping [1 ]
Qian, Yong [1 ]
Liu, Jiping [2 ]
机构
[1] Shanghai Jiao Tong Univ, Sch Chem & Chem Engn, Shanghai 200240, Peoples R China
[2] Beijing Inst Technol, Natl Lab Flame Retardant Mat, Sch Mat Sci & Engn, Beijing 100081, Peoples R China
基金
中国国家自然科学基金;
关键词
Polymer-matrix composites (PMCs); Hybrid; Thermal analysis; Thermosetting resin; THERMAL-STABILITY; GRAPHITE OXIDE; PHOSPHORUS; NANOCOMPOSITES; SILICON; FUNCTIONALIZATION; DEGRADATION; COMPOSITES; RESISTANCE; REDUCTION;
D O I
10.1016/j.compositesb.2013.12.033
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this paper, a novel graphene-based inorganic organic hybrid flame retardant (GFR) was prepared via sal gel reaction of FGO and phenyl-bis-(triethoxysilylpropyl) phosphamide (PBTP) and characterized by FT-IR, XPS, XRD, TGA and AFM. The influence of the GFR on the thermal stability and flame retardance of epoxy resin composites were characterized by TGA, LOI as well as micro-cone, which indicated that GFR brought a good effect in enhancing the residual char and flame retardance of epoxy composites. The dynamic mechanical properties and electrical properties of EP composites were also analyzed. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:341 / 349
页数:9
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