Analysis of hydrolysis reaction of N-phosphoryl phenylalanine by HPLC-ESI-Ms/MS

被引：0
|
作者：
Cao, SX
Zhang, JC
Xu, J
Liao, XC
Zhao, YF [1 ]
机构：
[1] Zhengzhou Univ, Dept Chem, Key Lab Chem Biol, Zhengzhou 450052, Peoples R China
[2] Tsing Hua Univ, Sch Life Sci & Engn, Dept Chem,Minist Educ, Key Lab Bioorgan Phosphorus Chem & Chem Biol, Beijing 100084, Peoples R China
来源：
CHINESE CHEMICAL LETTERS | 2004年 / 15卷 / 07期
关键词：
N-phosphoryl amino acids; hydrolysis reaction; HPLC-ESI-MS;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Hydrolysis procedure of N-phosphoryl phenylalanine (DIPP-Phe) was studied by HPLC-ESI-MS/MS. The results showed that (HO)(i-PrO)P(O)Phe was the main intermediate and the hydrolysis of DIPP-Phe also occurred through a penta-coordinate transition state.
引用
收藏
页码：817 / 820
页数：4
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