Performance of a direct detection camera for off-axis electron holography

被引:35
作者
Chang, Shery L. Y. [1 ,2 ,3 ]
Dwyer, Christian [1 ,2 ,4 ]
Barthel, Juri [1 ,2 ]
Boothroyd, Chris B. [1 ,2 ]
Dunin-Borkowski, Rafal E. [1 ,2 ]
机构
[1] Forschungszentrum Julich, Ernst Ruska Ctr Microscopy & Spect Electrons, D-52425 Julich, Germany
[2] Forschungszentrum Julich, Peter Grunberg Inst, D-52425 Julich, Germany
[3] Arizona State Univ, LeRoy Eyring Ctr Solid State Sci, Tempe, AZ 85287 USA
[4] Arizona State Univ, Dept Phys, Tempe, AZ 85287 USA
关键词
Electron holography; Direct detection camera; Phase error; DETECTION LIMITS; CRYO-EM; MICROSCOPY; IMPROVEMENT; NOISE;
D O I
10.1016/j.ultramic.2015.09.004
中图分类号
TH742 [显微镜];
学科分类号
摘要
The performance of a direct detection camera (DDC) is evaluated in the context of off-axis electron holographic experiments in a transmission electron microscope. Its performance is also compared directly with that of a conventional charge-coupled device (CCD) camera. The DDC evaluated here can be operated either by the detection of individual electron events (counting mode) or by the effective integration of many such events during a given exposure time (linear mode). It is demonstrated that the improved modulation transfer functions and detective quantum efficiencies of both modes of the DDC give rise to significant benefits over the conventional CCD cameras, specifically, a significant improvement in the visibility of the holographic fringes and a reduction of the statistical error in the phase of the reconstructed electron wave function. The DDC's linear mode, which can handle higher dose rates, allows optimisation of the dose rate to achieve the best phase resolution for a wide variety of experimental conditions. For suitable conditions, the counting mode can potentially utilise a significantly lower dose to achieve a phase resolution that is comparable to that achieved using the linear mode. The use of multiple holograms and correlation techniques to increase the total dose in counting mode is also demonstrated. (C) 2015 Published by Elsevier B.V.
引用
收藏
页码:90 / 97
页数:8
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