A new route for synthesis of spherical NiO nanoparticles via emulsion nano-reactors with enhanced photocatalytic activity

被引:100
作者
Fazlali, Farnaz [1 ]
Mahjoub, Ali Reza [1 ]
Abazari, Reza [1 ]
机构
[1] Tarbiat Modares Univ, Dept Chem, Tehran, Iran
关键词
Chemical synthesis; Nickel oxide photocatalyst; Emulsion nano-reactors; Homogeneous and spherical; Photocatalytic activity; NICKEL-OXIDE NANOPARTICLES; OPTICAL-PROPERTIES; NANOREACTORS MORPHOLOGY; FACILE; DECOMPOSITION; NANOSHEETS; CATALYSTS; FILMS;
D O I
10.1016/j.solidstatesciences.2015.08.022
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
This study has sought to draw a comparison among the nickel oxide nanostructures (NSs) with multiple shapes in terms of their photocatalytic properties. These NSs have been synthesized using a set of wet chemical methods (thermal-decomposition, sol-gel, hydrothermal, and emulsion nano-reactors), for which a similar precursor has been considered. For evaluation of the photocatalytic properties of the suggested NSs, methyl orange (MeO) solution photocatalytic degradation has been estimated based on UV-Vis spectroscopy. As shown by our results, the photocatalytic efficiency of the prepared NSs is highly dependent upon the shape of the corresponding structures. In this context, the emulsion nano-reactors (ENRs) method has been developed for the synthesis of pure nickel oxide nanoparticles (NPs) with unaggregated, quite spherical, and homogeneous NPs at environmental conditions. Compared with the other methods in this work, ENRs method shows high photocatalytic efficiency in the MeO dye decomposition. (C) 2015 Elsevier Masson SAS. All rights reserved.
引用
收藏
页码:263 / 269
页数:7
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