POST ANNEALING EFFECT ON STRUCTURAL AND OPTICAL PROPERTIES OF (α-Fe2O3) THIN FILMS PREPARED BY SPRAY PYROLYSIS WITH MOVING NOZZLE

被引：0

作者：

Meftah, Y. ^{[1
,2
]}

Bekker, D. ^{[2
]}

Benhaoua, B. ^{[1
,4
]}

Rahal, A. ^{[1
,2
,4
]}

Benhaoua, A. ^{[1
,2
,4
]}

Hamzaoui, A. H. ^{[3
]}

机构：

[1] Univ El Oued, Fac Technol, Lab VTRS, El Oued 39000, Algeria

[2] Univ El Oued, Fac Exact Sci, El Oued 39000, Algeria

[3] Ctr Natl Rech Sci Mat Tunisie, Soliman, Tunisia

[4] Unite Dev Energies Renouvelabes Zones Arides, El Oued 39000, Algeria

来源：

DIGEST JOURNAL OF NANOMATERIALS AND BIOSTRUCTURES | 2018年 / 13卷 / 02期

关键词：

Thin film; Hematite Fe2O3; Spray pyrolysis; Post annealing; X-ray diffraction; IRON-OXIDE NANOPARTICLES; HEMATITE; WATER; PERFORMANCE; DEPOSITION; REMOVAL; THICKNESS; SIZE; SOIL;

D O I：

暂无

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Hematite iron oxide (alpha-Fe2O3) thin films were prepared using spray pyrolysis with moving nozzle. Effects of 0-3 hours post heat treatment at 550 degrees C on their structural and optical properties have been studied. XRD analyses avowed the formation of hematite thin films structure along (104) and (110) as preferred orientations and intensities of which change with post annealing whereas the grain size was varied in 40-48 nm upon time heat treatment. SEM images showed that all sample having uniform morphology with variant shape upon post annealing time. The transparency of hematite thin films was averaged around 65% in the visible region, with an direct band gap in the range 2.11-2.13eV. FTIR study affirms the abundance of Fe-O bond in all samples. Results indicate that the best time of post-annealing was 2 hours.

引用

页码：465 / 474

页数：10

共 46 条

[11] Catalytic efficiency of iron oxides in decomposition of H2O2 for simultaneous NOX and SO2 removal: Effect of calcination temperature [J].

Ding, Jie ;

Zhong, Qin ;

Zhang, Shule .

JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2014, 393 :222-231

[12]

Fondell M., 2014, ACTA U UPSALIENSIS

[13] Growth and characterization of iron oxide nanocrystalline thin films via low-cost ultrasonic spray pyrolysis [J].

Goyal, Rajendra N. ;

Kaur, Davinder ;

Pandey, Ashish K. .

MATERIALS CHEMISTRY AND PHYSICS, 2009, 116 (2-3) :638-644

[14] Different responses of soil microbial metabolic activity to silver and iron oxide nanoparticles [J].

He, Shiying ;

Feng, Youzhi ;

Ni, Jun ;

Sun, Yufang ;

Xue, Lihong ;

Feng, Yanfang ;

Yu, Yingliang ;

Lin, Xiangui ;

Yang, Linzhang .

CHEMOSPHERE, 2016, 147 :195-202

[15] The impact of iron oxide magnetic nanoparticles on the soil bacterial community [J].

He, Shiying ;

Feng, Youzhi ;

Ren, Hongxuan ;

Zhang, Yu ;

Gu, Ning ;

Lin, Xiangui .

JOURNAL OF SOILS AND SEDIMENTS, 2011, 11 (08) :1408-1417

[16] Magnetic Nanoparticles: Surface Effects and Properties Related to Biomedicine Applications [J].

Issa, Bashar ;

Obaidat, Ihab M. ;

Albiss, Borhan A. ;

Haik, Yousef .

INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2013, 14 (11) :21266-21305

[17] Vibrational Spectroscopic Characterization of Hematite, Maghemite, and Magnetite Thin Films Produced by Vapor Deposition [J].

Jubb, Aaron M. ;

Allen, Heather C. .

ACS APPLIED MATERIALS & INTERFACES, 2010, 2 (10) :2804-2812

[18] Protective coating of superparamagnetic iron oxide nanoparticles [J].

Kim, DK ;

Mikhaylova, M ;

Zhang, Y ;

Muhammed, M .

CHEMISTRY OF MATERIALS, 2003, 15 (08) :1617-1627

[19] TiO2 and Fe2O3 Films for Photoelectrochemical Water Splitting [J].

Krysa, Josef ;

Zlamal, Martin ;

Kment, Stepan ;

Brunclikova, Michaela ;

Hubicka, Zdenek .

MOLECULES, 2015, 20 (01) :1046-1058

[20] Structural, optical, electrical and dielectrical properties of electrosynthesized nanocrystalline iron oxide thin films [J].

Kulkarni, SS ;

Lokhande, CD .

MATERIALS CHEMISTRY AND PHYSICS, 2003, 82 (01) :151-156

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