Synthesis and spectral characterization of some new azo dyes and their metal complexes

被引：35
作者：
Kilincarslan, Rafet
Erdem, Emin
Kocaokutgen, Hasan
机构：
[1] Pamukkale Univ, Dept Chem, Denizli, Turkey
[2] Ondokuz Mayis Univ, Dept Chem, TR-55139 Kurupelit, Samsun, Turkey
来源：
TRANSITION METAL CHEMISTRY | 2007年 / 32卷 / 01期
关键词：
D O I：
10.1007/s11243-006-0134-x
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A series of azo-metal chelate dyes have been synthesized by coupling substituted o-nitroaniline and p-t-/s-butylphenol. The spectral characterization of the azo dyes containing o-hydroxy group and azo-metal(II) chelate [metal(II): Cu, Ni, Co] dyes by IR spectra, UV-VIS spectra, NMR spectra, elemental analysis and magnetic susceptibility techniques are reported. The stoichiometry of the azo-metal chelates was determined by the spectroscopic titration method to be 1:2 (ML2).
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页码：102 / 106
页数：5
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