α-MnSe crystallites through solvothermal reaction in ethylenediamine

被引：26

作者：

Qin, T

Lu, J

Wei, S

Qi, PF

Peng, YY

Yang, ZP

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2002年 / 5卷 / 05期

基金：

中国国家自然科学基金;

关键词：

solvothermal; alpha-MnSe; crystallites; ethylenediamine;

D O I：

10.1016/S1387-7003(02)00387-8

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

alpha-MnSe crystallites were prepared by solvothermal reaction in ethylenediamine at 190 C. X-ray diffraction gave the a-MnSe phase of product, X-ray photoelectron spectroscopy indicated the valence state of Mn2+ and Se2-. The flaky morphology was found by the transmission electron microscope images. The optimal synthetic conditions were explored by using other nitrogen-containing solvents, and lowering the reaction temperature. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

收藏

页码：369 / 371

页数：3

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