Microstructural and Mechanical Characterization of Newly Developed Zn-Mg-CaO Composite

被引:3
作者
Pinc, Jan [1 ]
Kubasek, Jiri [2 ]
Drahokoupil, Jan [1 ]
Capek, Jaroslav [1 ]
Vojtech, Dalibor [2 ]
Skolakova, Andrea [1 ]
机构
[1] Czech Acad Sci, Inst Phys, Slovance 1999-2, Prague 18221, Czech Republic
[2] Univ Chem & Technol, Fac Chem Technol, Dept Met & Corros Engn, Tech 5, Prague 16628 6, Czech Republic
关键词
extrusion; biodegradable metals; zinc; EBSD; compressive properties; ball milling; powder metallurgy; mu CT; CORROSION PROPERTIES; DYNAMIC RECRYSTALLIZATION; PLASTIC-DEFORMATION; TEXTURE EVOLUTION; IN-VITRO; ALLOYS; PARTICLES; BEHAVIOR; VIVO;
D O I
10.3390/ma15238703
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this study, the Zn-0.8Mg-0.28CaO wt.% composite was successfully prepared using different conditions of ball milling (rotations and time) followed by a direct extrusion process. These materials were characterized from the point of view of microstructure and compressive properties, and the correlation between those characteristics was found. Microstructures of individual materials possessed differences in grain size, where the grain size decreased with the intensified conditions (milling speed and time). However, the mutual relation between grain size and compressive strength was not linear. This was caused by the effect of other factors, such as texture, intermetallic phases, and pores. Material texture affects the mechanical properties by a different activity ratio between basal and pyramidal slips. The properties of intermetallic particles and pores were determined in material volume using micro-computed tomography (mu CT), enhancing the precision of our assumptions compared with commonly applied methods. Based on that, and the analysis after the compressive tests, we were able to determine the influence of aspect ratio, feret diameters, and volume content of intermetallic phases and pores on mechanical behavior. The influence of the aspects on mechanical behavior is described and discussed.
引用
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页数:19
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