Recent advances in dispersive liquid-liquid microextraction for pesticide analysis

被引:143
作者
Ahmad, W. [1 ]
Al-Sibaai, A. A. [1 ]
Bashammakh, A. S. [1 ]
Alwael, H. [1 ]
El-Shahawi, M. S. [1 ]
机构
[1] King Abdulaziz Univ, Fac Sci, Dept Chem, Jeddah 21589, Saudi Arabia
关键词
Complex matrix; Dispersive liquid-liquid microextraction; Emerging pesticide; Green aspects; Nanotechnique; Pesticide analysis; Surface-modified electrode; Thin-layer stripping voltammetry; Trace analysis; Water analysis; MICELLAR ELECTROKINETIC CHROMATOGRAPHY; ENHANCED EMULSIFICATION MICROEXTRACTION; ENVIRONMENTAL WATER SAMPLES; ELECTRON CAPTURE DETECTION; DENSITY EXTRACTION SOLVENT; TANDEM MASS-SPECTROMETRY; FRUIT JUICE SAMPLES; GAS-CHROMATOGRAPHY; ORGANOPHOSPHORUS PESTICIDES; PHASE MICROEXTRACTION;
D O I
10.1016/j.trac.2015.04.022
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Dispersive liquid-liquid microextraction (DLLME) techniques have attracted considerable interest because they are cost effective, easy to operate, and reliably preconcentrate trace levels of analytes in complex matrices. This comprehensive review is concerned with principles, applications and developments of DLLME techniques for analysis of trace emerging pesticides in water. DLLME techniques have had few couplings to spectrofluorimetric methods and relatively none with electrochemical techniques. We highly recommend thin-layer stripping voltammetric techniques at surface-modified electrodes and spectrofluorimetric techniques coupled and implemented with DLLME. Great attention should be focused on developing low-cost, precise methods for analysis of trace concentrations of pesticides in various biological and environmental samples. We describe milestones and the combination of nanotechniques in the DLLME field, green aspects, advantages and shortcomings of known DLLME protocols. (C) 2015 Published by Elsevier B.V.
引用
收藏
页码:181 / 192
页数:12
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