Synthesis and structural investigation of 6,13-dichloroacylated tetraaza[14] annulene nickel(II) complexes

被引：11
|
作者：
Opozda, EM
Lasocha, W
机构：
[1] Jan Kochanowski Univ Humanities & Sci, Inst Chem, PL-25020 Kielce, Poland
[2] Jagiellonian Univ, Fac Chem, PL-30060 Krakow, Poland
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2000年 / 3卷 / 05期
关键词：
chloroacylation reactions; macrocyclic complexes; nickel(II) complexes; crystal structures;
D O I：
10.1016/S1387-7003(00)00048-4
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The reactions of the tetraaza[14] annulene Ni(II) complex (1) with chloroacyl chlorides afforded the 6,13-dichloroacylated complexes 2 and 3. By a demetallation procedure the metal free ligand of 2 was obtained. The crystal structure of the adduct 2 . C(6)H(5)CH(3), has been determined by the single-crystal X-ray diffraction method. (C) 2000 Elsevier Science S.A. All rights reserved.
引用
收藏
页码：239 / 242
页数：4
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