EFFICIENT MICROWAVE-ASSISTED SYNTHESES OF A SERIES OF NOVEL MONO(IMINO)PYRROLYL COMPOUNDS

被引：3
作者：
Su, Biyun [1 ]
Li, Xiaoteng [1 ]
Wang, Xudong [1 ]
Li, Qianding [1 ]
机构：
[1] Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Peoples R China
来源：
HETEROCYCLES | 2015年 / 91卷 / 10期
基金：
中国国家自然科学基金;
关键词：
Mono(imino)pyrrole; Microwave Chemistry; Crystal Structure; TRANSITION-METAL-COMPLEXES; ETHYLENE; LIGANDS; POLYMERIZATION; ACYLATION; CATALYSTS; PYRROLES; IRON;
D O I：
10.3987/COM-15-13265
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A series of novel mono(imino)pyrroles that were hard to prepare under traditional solvent reaction condition were readily synthesized under solvent free condition using microwave chemistry via p-TSA (p-toluenesulfonic acid) catalyzed Schiff base condensation. The structures of the compounds were characterized by means of MS, H-1 NMR, IR, elementary analysis and X-ray diffraction analysis. The reactivity of different aromatic amines with 2-acetylpyrrole was discussed.
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收藏
页码：1955 / 1963
页数：9
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