(E)-O-ethyl N-(4-nitrophenyl)thiocarbamate

被引：6
作者：
Benson, Ronald E.
Broker, Grant A.
Daniels, Lee M.
Tiekink, Edward R. T.
Wardell, James L.
Young, David J.
机构：
[1] Univ Texas, Dept Chem, San Antonio, TX 78249 USA
[2] Rigaku Amer Corp, The Woodlands, TX 77381 USA
[3] Griffith Univ, Eskitis Inst Cell & Mol Therapies, Nathan, Qld 4111, Australia
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷
关键词：
D O I：
10.1107/S1600536806033058
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C9H10N2O3S, is effectively planar, adopts an E conformation about the central C - N bond and exists in the thione form. N-H center dot center dot center dot S and C-H center dot center dot center dot O hydrogen bonds link the molecules into ribbons. Layers of ribbons are connected to adjacent layers via C-H center dot center dot center dot O interactions. The crystal is a non-merohedral twin, with the twin law describing a rotation of 180 degrees around the [100] direction.
引用
收藏
页码：O4106 / O4108
页数：3
相关论文
共 50 条
  • [21] N-{[(4-Nitrophenyl)amino]methyl}benzamide
    Buzarevski, Antonio
    Mikhova, Bozhana
    Popovski, Emil
    MOLBANK, 2014, (01)
  • [22] PROTECTIVE ACTION BY THIOURACIL AGAINST ACUTE TOXICITY IN MICE OF O-ETHYL O-(-4-NITROPHENYL) PHENYLPHOSPHONOTHIOATE (EPN)
    KELEMEN, MH
    VOLLE, RL
    TOXICOLOGY AND APPLIED PHARMACOLOGY, 1965, 7 (03) : 418 - &
  • [23] O-nucleophilicity of hydroxamate ions in reactions with ethyl 4-nitrophenyl ethylphosphonate, diethyl 4-nitrophenyl phosphate, and 4-nitrophenyl 4-toluenesulfonate
    Simanenko, YS
    Prokop'eva, TM
    Popov, AF
    Bunton, CA
    Karpichev, EA
    Savelova, VA
    Ghosh, KK
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2004, 40 (09) : 1337 - 1350
  • [24] O-nucleophilicity of hydroxamate ions in reactions with ethyl 4-nitrophenyl ethylphosphonate, diethyl 4-nitrophenyl phosphate, and 4-nitrophenyl 4-toluenesulfonate
    Yu. S. Simanenko
    T. M. Prokop’eva
    A. F. Popov
    C. A. Bunton
    E. A. Karpichev
    V. A. Savelova
    K. K. Ghosh
    Russian Journal of Organic Chemistry, 2004, 40 : 1337 - 1350
  • [25] (E)-O-methyl N-(4-methylphenyl)thiocarbamate
    Ho, Soo Yei
    Kuan, Fong Sheen
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O1723 - O1724
  • [26] STEPWISE MECHANISMS OF THE AMINOLYSES OF 4-NITROPHENYL AND 2,4-DINITROPHENYL O-ETHYL DITHIOCARBONATES IN AQUEOUS-ETHANOL
    CASTRO, EA
    MUNOZ, G
    SALAS, M
    SANTOS, JG
    INTERNATIONAL JOURNAL OF CHEMICAL KINETICS, 1995, 27 (10) : 987 - 995
  • [27] O-ETHYL-O-(4-NITROPHENYL)BENZENE PHOSPHONOTHIOATE (EPN)
    GIFKINS, MR
    JACOBSON, RA
    CRYSTAL STRUCTURE COMMUNICATIONS, 1980, 9 (02): : 571 - 574
  • [28] N-(4-nitrophenyl)-trans-2-aminocyclohexanol
    Chinnakali, K
    Fun, HK
    Sriraghavan, K
    Ramakrishnan, VT
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 1865 - 1867
  • [29] Bis[N-(4-nitrophenyl)thiobenzamidato]mercury(II)
    Habibi, Mohammad Hossein
    Tangestaninejad, Shahram
    Fallah-Shojaie, Abdollah
    Mohammadpoor-Baltork, Iraj
    Mokhtari, Reza
    Brooks, Neil R.
    Clegg, William
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2007, 63 : M494 - M495
  • [30] Surface and aggregation properties of N-(4-nitrophenyl)perfluorononanamide
    Granados, AM
    Fidelio, GD
    deRossi, RH
    LANGMUIR, 1997, 13 (15) : 4079 - 4084
12345