New glassware for small-scale distillation

被引：1

作者：

Petroski, RJ ^{[1
]}

Bowe, HJ ^{[1
]}

机构：

[1] ACE GLASS INC MANUFACTURERS, VINELAND, NJ 08360 USA

来源：

SYNTHETIC COMMUNICATIONS | 1996年 / 26卷 / 18期

关键词：

D O I：

10.1080/00397919608003746

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Distillation of less than a mi of sample can be accomplished with a jacketed Hickman still. The jacket allows positioning of a coolant such as dry ice/acetone at the site of desired condensation. A jacketed distillation head will accommodate samples up to a volume of 3 mi. Distillate is easily removed with a Pasteur pipette. Details of the glassware design are given.

引用

页码：3421 / 3424

页数：4