Recent Advances in the Post-Column Derivatization for the Determination of Mycotoxins in Food Products and Feed Materials by Liquid Chromatography and Fluorescence Detection

被引：11
|
作者：
Nardiello, Donatella [1 ]
Lo Magro, S. [2 ]
Iammarino, M. [2 ]
Palermo, Carmen [1 ]
Muscarella, Marilena [2 ]
Centonze, Diego [1 ]
机构：
[1] Univ Foggia, Dipartimento Sci Agr Alimenti & Ambiente, I-7121 Foggia, Italy
[2] Ist Zooprofilatt Sperimentale Puglia & Basilicata, I-71100 Foggia, Italy
来源：
CURRENT ANALYTICAL CHEMISTRY | 2014年 / 10卷 / 03期
关键词：
Aflatoxins; fumonisins; fluorescence detection; DON; liquid chromatography; method validation; NIV; postcolumn derivatization; IMMUNOAFFINITY COLUMN CLEANUP; MASS-SPECTROMETRIC METHOD; SOLID-PHASE DISPERSION; PHOTOCHEMICAL DERIVATIZATION; TRICHOTHECENE MYCOTOXINS; FLUOROMETRIC DETECTION; DEOXYNIVALENOL DON; FUSARIUM TOXINS; FUMONISINS B-1; OCHRATOXIN-A;
D O I：
10.2174/1573411010999131219102253
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The problems and risks associated with mycotoxin contamination of foods and feedstuffs have led to the development of a variety of confirmatory analytical methods for their determination, based on chromatographic techniques and capillary electrophoresis. In this paper, an overview of the analytical methods developed in the last decade and based on post-column derivatization coupled with high-performance liquid chromatography and fluorescence detection is reported. A particular focus on the determination of aflatoxins (B1, B2, G1 and G2), fumonisins (B1 and B2) and trichotecenes deoxynivalenol (DON) and nivalenol (NIV) in cereals products for human and animal consumption is given. Important aspects as the optimization of the experimental conditions and validation of the analytical methods are also described.
引用
收藏
页码：355 / 365
页数：11
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