(E)-2-(Isonicotinoylhydrazonomethyl)benzoic acid methanol monosolvate

被引:0
作者
Li, Wenkuan
Yin, Handong
Wen, Liyuan
Cui, Jichun
Wang, Daqi
机构
[1] College of Chemistry and Chemical Engineering, Liaocheng University
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
D O I
10.1107/S1600536809038902
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C14H11N3O3 center dot CH4O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formylbenzoic acid in methanol. The hydrazone molecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04 (5)degrees. In the crystal structure, molecules are linked by O-H center dot center dot center dot N, O-H center dot center dot center dot O and N-H center dot center dot center dot O hydrogen-bonding interactions.
引用
收藏
页码:O2578 / +
页数:8
相关论文
共 5 条
  • [1] [Anonymous], 1996, SMART SAINT
  • [2] Hydrazone as complexing agent: Synthesis, structural characterization and biological studies of some complexes
    Dhande, V. V.
    Badwaik, V. B.
    Aswar, A. S.
    [J]. RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2007, 52 (08) : 1206 - 1210
  • [3] Sheldrick G.M., 1996, SADABS
  • [4] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [5] (E)-N′-(3,4-Dimethoxybenzylidene)-2,4-dihydroxybenzohydrazide methanol solvate
    Zhang, Qiao-Ling
    Yin, Zi
    Deng, Xu-Ming
    Liu, Song-Cai
    Song, De-Guang
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2392 - +