Vertically aligned carbon nanofiber nanoelectrode arrays: electrochemical etching and electrode reusability

被引:10
作者
Gupta, Rakesh K. [1 ,2 ]
Meyyappan, M. [2 ]
Koehne, Jessica E. [2 ]
机构
[1] GGM Sci Coll, Dept Elect, Jammu 180004, J&K, India
[2] NASA, Ames Res Ctr, Moffett Field, CA 94035 USA
关键词
LABEL-FREE DETECTION; FABRICATION; BIOSENSOR; SENSORS;
D O I
10.1039/c4ra01779j
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Vertically aligned carbon nanofibers in the form of nanoelectrode arrays were grown on nine individual electrodes, arranged in a 3 x 3 array geometry, in a 6.25 cm(2) chip. Electrochemical etching of the carbon nanofibers was employed for electrode activation and enhancing the electrode kinetics. Here, we report the effects of electrochemical etching on the fiber height and electrochemical properties. Electrode regeneration by amide hydrolysis and electrochemical etching is also investigated for electrode reusability.
引用
收藏
页码:22642 / 22650
页数:9
相关论文
共 33 条
[1]  
[Anonymous], 2001, ELECTROCHEMICAL METH
[2]   Nanoelectrodes, nanoelectrode arrays and their applications [J].
Arrigan, DWM .
ANALYST, 2004, 129 (12) :1157-1165
[3]   Vertically aligned carbon nanofiber electrode arrays for nucleic acid detection [J].
Arumugam, Prabhu U. ;
Yu, Edmond ;
Riviere, Roger ;
Meyyappan, M. .
CHEMICAL PHYSICS LETTERS, 2010, 499 (4-6) :241-246
[4]   Wafer-scale fabrication of patterned carbon nanofiber nanoelectrode arrays: A route for development of multiplexed, ultrasensitive disposable biosensors [J].
Arumugam, Prabhu U. ;
Chen, Hua ;
Siddiqui, Shabnam ;
Weinrich, Jarret A. P. ;
Jejelowo, Ayodeji ;
Li, Jun ;
Meyyappan, M. .
BIOSENSORS & BIOELECTRONICS, 2009, 24 (09) :2818-2824
[5]   Electrocatalysis at graphite and carbon nanotube modified electrodes: edge-plane sites and tube ends are the reactive sites [J].
Banks, CE ;
Davies, TJ ;
Wildgoose, GG ;
Compton, RG .
CHEMICAL COMMUNICATIONS, 2005, (07) :829-841
[6]   An optimised electrochemical biosensor for the label-free detection of C-reactive protein in blood [J].
Bryan, Thomas ;
Luo, Xiliang ;
Bueno, Paulo R. ;
Davis, Jason J. .
BIOSENSORS & BIOELECTRONICS, 2013, 39 (01) :94-98
[7]   SILICON QUANTUM WIRE ARRAY FABRICATION BY ELECTROCHEMICAL AND CHEMICAL DISSOLUTION OF WAFERS [J].
CANHAM, LT .
APPLIED PHYSICS LETTERS, 1990, 57 (10) :1046-1048
[8]   Nanomaterials based electrochemical sensors for biomedical applications [J].
Chen, Aicheng ;
Chatterjee, Sanghamitra .
CHEMICAL SOCIETY REVIEWS, 2013, 42 (12) :5425-5438
[9]   Applications of silicon nanowires functionalized with palladium nanoparticles in hydrogen sensors [J].
Chen, Z. H. ;
Jie, J. S. ;
Luo, L. B. ;
Wang, H. ;
Lee, C. S. ;
Lee, S. T. .
NANOTECHNOLOGY, 2007, 18 (34)
[10]   Immunoassays based on electrochemical detection using microelectrode arrays [J].
Dill, K ;
Montgomery, DD ;
Ghindilis, AL ;
Schwarzkopf, KR ;
Ragsdale, SR ;
Oleinikov, AV .
BIOSENSORS & BIOELECTRONICS, 2004, 20 (04) :736-742