Crystal structure of catena-poly[(μ2-4,4′-bipyridyl-κN,N′-bis(O,O′-dimethyldithiophosphato-κS)-zinc(II)], {C14H20N2O4P2S4Zn}n

被引:3
作者
Tan, Yee Seng [1 ]
Tiekink, Edward R. T. [1 ]
机构
[1] Sunway Univ, Sch Sci & Technol, Res Ctr Crystalline Mat, Bandar Sunway 47500, Selangor Darul, Malaysia
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2019年 / 234卷 / 04期
关键词
DITHIOPHOSPHATES; ADDUCTS; ZINC;
D O I
10.1515/ncrs-2019-0085
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C14H20N2O4P2S4Zn, triclinic, P (1) over bar (no. 2), a = 8.0014(2) angstrom, b = 10.3376(2) angstrom, c =14.2488(3) angstrom, alpha = 84.676(2)degrees , beta = 76.042(2)degrees, gamma = 79.752(2)degrees , V = 1124.01(4) angstrom(3), Z = 2, R-gt(F) = 0.0265, wR(ref)(F-2) = 0.0655, T = 100(2) K.
引用
收藏
页码:743 / 745
页数:3
相关论文
共 10 条
[1]  
Agilent Technologies, 2017, CRYSALIS PRO
[2]   Supramolecular aggregation in diimine adducts of zinc(II) dithiophosphates: controlling the formation of monomeric, dimeric, polymeric (zig-zag and helical), and 2-D motifs [J].
Chen, DL ;
Lai, CS ;
Tiekink, ERT .
CRYSTENGCOMM, 2006, 8 (01) :51-58
[3]   WinGX and ORTEP for Windows: an update [J].
Farrugia, Louis J. .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2012, 45 :849-854
[4]   Synthesis and polymer structure of [Zn(4,4′-bipy){(i-PrO)2PS2}2]n and thermal properties of ZnL{(i-PrO)2PS2}2 (L = phen, 2,2′-bipy, 4,4′-bipy) [J].
Glinskaya, LA ;
Shchukin, VG ;
Klevtsova, RF ;
Mazhara, AP ;
Larionov, SV .
JOURNAL OF STRUCTURAL CHEMISTRY, 2000, 41 (04) :632-639
[5]   Steric control over polymer formation and topology in adducts of zinc dithiophosphates formed with bridging bipyridine ligands [J].
Lai, CS ;
Liu, S ;
Tiekink, ERT .
CRYSTENGCOMM, 2004, 6 :221-226
[6]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[7]  
Sheldrick GM, 2015, ACTA CRYSTALLOGR C, V71, P3, DOI [10.1107/S2053229614024218, 10.1107/S2053273314026370, 10.1107/S0108767307043930]
[8]   Exploring the Topological Landscape Exhibited by Binary Zinc-triad 1,1-dithiolates [J].
Tiekink, Edward R. T. .
CRYSTALS, 2018, 8 (07)
[9]   Perplexing Coordination Behaviour of Potentially Bridging Bipyridyl-Type Ligands in the Coordination Chemistry of Zinc and Cadmium 1,1-Dithiolate Compounds [J].
Tiekink, Edward R. T. .
CRYSTALS, 2018, 8 (01)
[10]   catena-poly[bis(O,O'-diethyldithiophosphato-S)zinc(II)-mu-4,4'-bipyridyl-N:N'] [J].
Zhu, DL ;
Yu, YP ;
Guo, GC ;
Zhuang, HH ;
Huang, JS ;
Liu, Q ;
Xu, Z ;
You, XZ .
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 :1963-1966