Synthesis and crystal structure of a new A type pyridine iodide

被引：0

作者：

Zhang, Y

Wu, JY

Yu, WT

Tian, YP ^{[1
]}

Jiang, MH

机构：

[1] Fuyang Normal Sch, Dept Chem, Fuyang 236032, Peoples R China

[2] Anhui Univ, Dept Chem, Hefei 230039, Peoples R China

[3] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Peoples R China

[4] Nanjing Univ, State Key Lab Coordinat Chem, Nanjing 210093, Peoples R China

来源：

CHINESE JOURNAL OF INORGANIC CHEMISTRY | 2002年 / 18卷 / 10期

关键词：

A type pyriding iodide; synthesig; crystal structure;

D O I：

暂无

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A new A type pyriding iodide was synthesized by reaction of 4-picoline and methyl diiodide. The structure was characterized by elemental analysis, IR, UV and TG. The crystal structure of the title compound was determined by X-ray single crystal diffraction. The crystal belongs to monoclinic with space group C2/c, a = 18. 812(4) Angstrom, b = 8.7816 (6) Angstrom, c = 10.3165 (12) Angstrom, 6 = 93.71 (1), Angstrom = 1700.7 (4) Angstrom, Z = 4. In the molecule, two 4-picoline molecules are bonded by -CH2 group to form A type pyridine salt.

引用

页码：1020 / 1022

页数：3

共 11 条

[1]

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[2]

2-M

[3]

INGRID GVM, 1997, J PHYS CHEM-US, V101, P7265

[4]

INGRID GVM, 1996, J AM CHEM SOC, V118, P12830