2,2′-Diamino-4,4′-bi-1,3-thiazolium bis(3-nitrobenzoate)

被引：1

作者：

Liu, Bing-Xin ^{[1
]}

Yu, Yan-Ping ^{[1
]}

Lin, Yuan-Yuan ^{[1
]}

Du, Mei ^{[1
]}

机构：

[1] Shanghai Univ, Dept Chem, Shanghai 200444, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809005856

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title salt, C6H8N4S22+center dot 2C(7)H(4)NO(4)(-), the diprotonated diaminobithiazole dication is located on an inversion center. The carboxylate group of the anion is twisted with respect to the benzene ring, with a dihedral angle of 13.6 (4)degrees. N-H center dot center dot center dot O hydrogen bonds involving the amino and ammonium groups of the dication and the carboxylate functionality of the anion generate supramolecular chains in the crystal.

引用

页码：O590 / U2425

页数：9

共 12 条

[1] COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92 [J].

ALTOMARE, A ;

CASCARANO, G ;

GIACOVAZZO, C ;

GUAGLIARDI, A .

JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) :343-350

[2]

[Anonymous], 2004, APEX2 SAINT

[3]

Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI [DOI 10.1107/S0021889812029111, DOI 10.1107/S0021889899006020]

[4]

Farrujia LJ., 1997, J APPL CRYSTALLOGR, V30, P565, DOI [10.1107/S0021889897003117, DOI 10.1107/S0021889897003117]

[5] INTERACTION OF BLEOMYCIN A-2 WITH DEOXYRIBONUCLEIC-ACID - DNA UNWINDING AND INHIBITION OF BLEOMYCIN-INDUCED DNA BREAKAGE BY CATIONIC THIAZOLE AMIDES RELATED TO BLEOMYCIN A-2 [J].

FISHER, LM ;

KURODA, R ;

SAKAI, TT .

BIOCHEMISTRY, 1985, 24 (13) :3199-3207

[6]

Higashi T., 1995, ABSCOR

[7] 2,2′-Diamino-4,4′-bi-1,3-thiazol-3,3′-diium bis(2,2′-diamino-4,4′-bi-1,3-thiazol-3-ium) tetrakis(2-nitrobenzoate) [J].

Liu, BX ;

Yu, JY ;

Xu, DJ .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 :O4119-O4120

[8] 2,2′-Diamino-4,4′-bi-1,3-thiazole [J].

Liu, JG ;

Xu, DJ ;

Hung, CH .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2003, 59 :O312-O313

[9] A short history of SHELX [J].

Sheldrick, George M. .

ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122

[10]

Sun WL, 1997, J APPL POLYM SCI, V64, P2309, DOI 10.1002/(SICI)1097-4628(19970620)64:12<2309::AID-APP6>3.3.CO

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