Optimization of the capillary gas chromatographic analysis of mono- and oligosaccharides in honeys

被引：13
|
作者：
Bárez, JAG [1 ]
Garcia-Villanova, RJ [1 ]
Garcia, SE [1 ]
Paramás, AMG [1 ]
机构：
[1] Univ Salamanca, Fac Farm, Dept Quim Analit Nutr & Bromatol, E-37007 Salamanca, Spain
来源：
CHROMATOGRAPHIA | 1999年 / 50卷 / 7-8期
关键词：
gas chromatography; honey sugars; oxime-trimethylsilyl ethers of sugars; mono-; di and trisaccharides;
D O I：
10.1007/BF02490743
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A capillary gas chromatographic method has been developed for simultaneous determination of at least 18 sugars (2 monosaccharides, 11 disaccharides and 5 trisaccharides) in honey, as their oxime-trimethylsilyl ethers. The chromatographic conditions have been systematically and thoroughly optimized, to eliminate the peak overlap commonly reported for this and other methods, especially for disaccharides. Complete analytical details are reported.
引用
收藏
页码：461 / 469
页数：9
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