Influence of titanium on nano-cluster (Y, Ti, O) stability in ODS ferritic materials

被引:114
作者
Ratti, M. [1 ]
Leuvrey, D. [1 ]
Mathon, M. H. [2 ]
de Carlan, Y. [1 ]
机构
[1] CEA Saclay, Serv Rech Met Appl, F-91191 Gif Sur Yvette, France
[2] CEA Saclay, Lab Leon Brillouin, CNRS, CEA, F-91191 Gif Sur Yvette, France
关键词
MARTENSITIC STEELS; DISPERSION; ALLOYS; PARTICLES;
D O I
10.1016/j.jnucmat.2008.12.171
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The addition of titanium is well known to refine the precipitation of nano-phases (Y, Ti, 0) in oxide dispersion strengthened (ODS) ferritic materials. In order to understand the influence of titanium on the nano-cluster nucleation, two powders of ferritic materials Fe-18Cr-1W were mechanically alloyed with a nano-powder of yttrium oxide Y(2)O(3) in a planetary mill, one without titanium and one with 0.8 wt% of titanium. Several analyses were conducted by small angle neutron scattering (SANS) on powders after different milling conditions and heat treatments. The SANS technique appeared to be extremely useful to follow the precipitation of the nano-phases in ODS ferritic materials. The analysis of these tests indicates that the role played by titanium is clearly observed during the reprecipitation of the nano-oxides though the effect of titanium on the oxide dissolution during the milling is not obvious. Titanium is usually considered to refine the precipitation in ODS materials. This study shows that the nano-phases formed in powders with some titanium are much more resistant to the coarsening than the phases formed without titanium. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:540 / 543
页数:4
相关论文
共 16 条
[1]   Mechanical dispersion of Y2O3 nanoparticles in steel EUROFER 97:: process and optimisation [J].
de Castro, V ;
Leguey, T ;
Monge, MA ;
Muñoz, A ;
Pareja, R ;
Amador, DR ;
Torralba, JM ;
Victoria, M .
JOURNAL OF NUCLEAR MATERIALS, 2003, 322 (2-3) :228-234
[2]   Recent results of the reduced activation ferritic/martensitic steel development [J].
Jitsukawa, S ;
Kimura, A ;
Kohyama, A ;
Klueh, RL ;
Tavassoli, AA ;
van der Schaaf, B ;
Odette, GR ;
Rensman, JW ;
Victoria, M ;
Petersen, C .
JOURNAL OF NUCLEAR MATERIALS, 2004, 329 :39-46
[3]   TEM characterization of structure and composition of nanosized ODS particles in reduced activation ferritic-martensitic steels [J].
Klimiankou, M ;
Lindau, R ;
Möslang, A .
JOURNAL OF NUCLEAR MATERIALS, 2004, 329 :347-351
[4]   Oxide dispersion-strengthened steels: A comparison of some commercial and experimental alloys [J].
Klueh, RL ;
Shingledecker, JP ;
Swindeman, RW ;
Hoelzer, DT .
JOURNAL OF NUCLEAR MATERIALS, 2005, 341 (2-3) :103-114
[5]   Ferritic/martensitic steels - overview of recent results [J].
Klueh, RL ;
Gelles, DS ;
Jitsukawa, S ;
Kimura, A ;
Odette, GR ;
van der Schaaf, B ;
Victoria, M .
JOURNAL OF NUCLEAR MATERIALS, 2002, 307 (1 SUPPL.) :455-465
[6]   Three-dimensional atom probe observation of nanoscale titanium-oxygen clustering in an oxide-dispersion-strengthened Fe-12Cr-3W-0.4Ti+Y2O3 ferritic alloy [J].
Larson, DJ ;
Maziasz, PJ ;
Kim, IS ;
Miyahara, K .
SCRIPTA MATERIALIA, 2001, 44 (02) :359-364
[7]   Mechanical and microstructural properties of a hipped RAFM ODS-steel [J].
Lindau, R ;
Möslang, A ;
Schirra, M ;
Schlossmacher, P ;
Klimenkov, M .
JOURNAL OF NUCLEAR MATERIALS, 2002, 307 (1 SUPPL.) :769-772
[8]   A SANS investigation of the irradiation-enhanced α-α′ phases separation in 7-12 Cr martensitic steels [J].
Mathon, MH ;
de Carlan, Y ;
Geoffroy, G ;
Averty, X ;
Alamo, A ;
de Novion, CH .
JOURNAL OF NUCLEAR MATERIALS, 2003, 312 (2-3) :236-248
[9]   From intensity to structure of materials [J].
Mathon, MH ;
de Novion, CH .
JOURNAL DE PHYSIQUE IV, 1999, 9 (P1) :127-146
[10]  
MATHON MH, 1995, THESIS ORSAY U PARIS