In-situ observation of intragranular ferrite nucleation at oxide particles

被引:29
作者
Hanamura, T
Shibata, H
Waseda, Y
Nakajima, H
Torizuka, S
Takanashi, T
Nagai, K
机构
[1] Natl Res Inst Met, Tsukuba, Ibaraki 3050047, Japan
[2] Tohoku Univ, Inst Adv Mat Proc, Aoba Ku, Sendai, Miyagi 9808577, Japan
关键词
in-situ observation; austenite-ferrite phase transformation; confocal scanning laser microscope; oxide; MnS; TiN;
D O I
10.2355/isijinternational.39.1188
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
In-situ real time observation of the ferrite nucleation at nonmetallic inclusions has been successfully made at elevated temperatures with a confocal scanning laser microscope. The nucleation site, nucleation temperature, and/morphological change of the precipitates and ferrite can be sequentially determined as the phenomena occurring on the surface of steel. A polygonal ferrite starts to precipitate at an oxide particle at 1 010 K and a Widmanstatten ferrite starts to precipitate at a MnS particle at 967 K. The degree of super cooling for austenite-ferrite transformation is found to be in good agreement with the prediction by a thermodynamic calculation.
引用
收藏
页码:1188 / 1193
页数:6
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