Microwave-assisted metathesis synthesis of Schoenfliesite-type MSn(OH)6 (M = Mg, Ca, Zn, and Sr) materials

被引：27
|
作者：
Kramer, Jonathan W. [1 ,2 ]
Isaacs, Steven A. [1 ,2 ]
Manivannan, Venkatesan [1 ,2 ]
机构：
[1] Colorado State Univ, Dept Mech Engn, Ft Collins, CO 80523 USA
[2] Colorado State Univ, Dept Chem, Ft Collins, CO 80523 USA
来源：
JOURNAL OF MATERIALS SCIENCE | 2009年 / 44卷 / 13期
关键词：
SOLID-STATE SYNTHESIS; PEROVSKITE OXIDES; ION BATTERIES; TIN; ROUTE; NANOSTRUCTURES; ZIRCONIUM; CAPACITY;
D O I：
10.1007/s10853-009-3448-1
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Technologically important Schoenfliesite type MSn(OH)(6) (M = Mg, Ca, Zn, and Sr) materials were synthesized by a simple solid state metathesis (SSM) approach, assisted by microwave energy. The SSM nature of the reaction is strongly suggested by the formation of NaCl byproduct. The synthesized materials are characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), thermo gravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), and diffuse reflectance (DR) in the UV-VIS range, to determine physical properties and establish structure-property relationships for these materials.
引用
收藏
页码：3387 / 3392
页数：6
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