Analysis of brominated dioxins and furans by high resolution gas chromatography/high resolution mass spectrometry

被引：27
|
作者：
Hagberg, Jessika [1 ]
机构：
[1] Univ Orebro, Sch Sci & Technol, MTM Res Ctr, S-70182 Orebro, Sweden
来源：
JOURNAL OF CHROMATOGRAPHY A | 2009年 / 1216卷 / 03期
关键词：
Brominated dibenzo-p dioxins and furans; PBDD/Fs; Clean-up; Analysis; Review; DIBENZO-P-DIOXINS; POLYBROMINATED DIPHENYL ETHERS; FLAME RETARDANTS; DECABROMODIPHENYL ETHER; FLY-ASH; PBDD/F; JAPAN; MUNICIPAL; PRODUCTS; PCDD/F;
D O I：
10.1016/j.chroma.2008.10.022
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
This article reviews the available literature on the analysis of brominated dibenzo-p dioxins and furans (PBDD/Fs) by high resolution gas chromatography/high resolution mass spectrometry (HRGC/HRMS). Sample extraction and clean up, injection techniques, chromatographic separation, labelled standards and QA/QC works are discussed. Furthermore, full separation of PBDD/Fs from polybrominated diphenyl ethers (PBDEs) during clean up and control of possible chromatographic interference of PBDEs (luring instrumental analysis as well as possible actions to further enhance the quality of published data are discussed in detail. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码：376 / 384
页数：9
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