2-Bromo-N′-[(Z)-2-bromobenzylidene]-5-methoxybenzohydrazide

被引：2

作者：

Li, Hongqi ^{[1
]}

Sarojini, B. K. ^{[2
]}

Narayana, B. ^{[3
]}

Yathirajan, H. S. ^{[4
]}

Harrison, William T. A. ^{[5
]}

机构：

[1] Donghua Univ, Key Lab Sci & Technol Ecotext, Minist Educ, Coll Chem Chem Engn & Biotechnol, Shanghai 201620, Peoples R China

[2] PA Coll Engn, Dept Chem, Mangalore 574153, India

[3] Mangalore Univ, Dept Studies Chem, Mangalagangothri 574199, Karnataka, India

[4] Univ Mysore, Dept Studies Chem, Mysore 570006, Karnataka, India

[5] Univ Aberdeen, Dept Chem, Aberdeen AB24 3UE, Scotland

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

关键词：

D O I：

10.1107/S1600536809024921

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C15H12Br2N2O2, the molecule adopts an E conformation about the C = N double bond and a transoid conformation about the central N-N bond, with a C(= O)-N-N-C(H) dihedral angle of 169.4 (4)degrees. In the crystal, molecules are linked by N-H center dot center dot center dot O hydrogen bonds, leading to C(4) chains. The packing also features slipped pi-pi stacking interactions, with a centroid-centroid separation of 3.838 (3) angstrom and a slippage of 1.19 angstrom.

引用

页码：O1750 / U2024

页数：10

共 4 条

[1] [Anonymous], SMART SAINT SADABS
[2] 2-Bromo-N′-[(E)-4-chlorobenzylidene]-5-methoxybenzohydrazide
Butcher, Ray J.
Jasinski, Jerry P.
Narayana, B.
Sunil, K.
Yathirajan, H. S.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3652 - U4858
[3] 2-Bromo-5-methoxy-N′-[(E)-(4-nitrophenyl)methylene]benzohydrazide
Narayana, B.
Siddaraju, B. P.
Raju, C. R.
Yathirajan, H. S.
Bolte, Michael
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3522 - U3617
[4] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122

← 1 →