Preparation of potato starch-based carbon particles by low-temperature carbonization in oil

被引：7

作者：

Xue, Zhonghua ^{[1
,2
]}

Chen, Peirong ^{[1
,3
]}

He, Lifang ^{[1
]}

Zhang, Zhi ^{[1
,2
]}

Yang, Qi ^{[1
]}

Cheng, Beijiu ^{[3
]}

机构：

[1] Anhui Agr Univ, Sch Sci, Dept Appl Chem, Hefei 230036, Anhui, Peoples R China

[2] Hefei Univ Technol, Sch Chem & Chem Engn, Dept Chem Proc, Hefei, Peoples R China

[3] Anhui Agr Univ, Dept Educ, Key Lab Biomass & Energy, Hefei 230036, Anhui, Peoples R China

来源：

INTERNATIONAL JOURNAL OF MATERIALS RESEARCH | 2015年 / 106卷 / 11期

关键词：

Carbon particles; Starch; Microstructure; UNIFORM MESOPOROUS CARBON; HYDROTHERMAL CARBONIZATION; NANOPARTICLES; SPHERES;

D O I：

10.3139/146.111295

中图分类号：

TF [冶金工业];

学科分类号：

0806 ;

摘要：

Potato starch-based carbon particles were prepared by low-temperature carbonization in methyl silicone oil at 220 degrees C for 15 h and subsequent carbonization at 600 degrees C for 1 hour under nitrogen. The as-prepared carbon particles were molded, and then heat-treated. The results confirmed that carbon particles could keep the original shape of the potato starch and exhibit high monodispersity with smooth surfaces. The size distribution of carbon particles ranged from 10 to 100 pm and the blocks molded from the carbon particles exhibited relatively superior mechanical strength with a flexural strength of 85.7 MPa. Additionally, it was found that the low-temperature carbonization in oil is crucial in the preparation of this kind of carbon particle.

引用

页码：1196 / 1201

页数：6

共 14 条

[1] Fe3 O4 Nanoparticles Embedded in Uniform Mesoporous Carbon Spheres for Superior High- Rate Battery Applications [J].

Chen, Yu ;

Song, Bohang ;

Li, Meng ;

Lu, Li ;

Xue, Junmin .

ADVANCED FUNCTIONAL MATERIALS, 2014, 24 (03) :319-326

[2] Structural effects of iron oxide nanoparticles and iron ions on the hydrothermal carbonization of starch and rice carbohydrates [J].

Cui, XJ ;

Antonietti, M ;

Yu, SH .

SMALL, 2006, 2 (06) :756-759

[3] Effect of additives on mechanical properties of oxidation-resistant carbon/carbon composite fabricated by rapid CVD method [J].

Luo, RY ;

Yang, Z ;

Li, LF .

CARBON, 2000, 38 (15) :2109-2115

[4] Catalytic chemical vapour deposition synthesis of carbon spheres [J].

Mehraban, Zahra ;

Farzaneh, Faezeh ;

Dadmehr, Vahid .

MATERIALS LETTERS, 2009, 63 (20) :1653-1655

[5] Hollow nitrogen-doped carbon spheres as efficient and durable electrocatalysts for oxygen reduction [J].

Sanetuntikul, Jakkid ;

Hang, Tao ;

Shanmugam, Sangaraju .

CHEMICAL COMMUNICATIONS, 2014, 50 (67) :9473-9476

[6] Chemical and Structural Properties of Carbonaceous Products Obtained by Hydrothermal Carbonization of Saccharides [J].

Sevilla, Marta ;

Fuertes, Antonio B. .

CHEMISTRY-A EUROPEAN JOURNAL, 2009, 15 (16) :4195-4203

[7] Carbon/graphite seal materials prepared from mesocarbon microbeads [J].

Song, YZ ;

Zhai, GT ;

Li, GS ;

Shi, JL ;

Guo, QG ;

Liu, L .

CARBON, 2004, 42 (8-9) :1427-1433

[8] Chemistry and materials options of sustainable carbon materials made by hydrothermal carbonization [J].

Titirici, Maria-Magdalena ;

Antonietti, Markus .

CHEMICAL SOCIETY REVIEWS, 2010, 39 (01) :103-116

[9] Functional Hollow Carbon Nanospheres by Latex Templating [J].

White, Robin J. ;

Tauer, Klaus ;

Antonietti, Markus ;

Titirici, Maria-Magdalena .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2010, 132 (49) :17360-17363

[10] Effects of low-temperature carbonization temperature and time on morphology of carbon particles from maize starch [J].

Xue, Zhonghua ;

Chen, Peirong ;

Yang, Qi ;

He, Lifang ;

Mu, Shuhui ;

Cheng, Beijiu .

JOURNAL OF MATERIALS SCIENCE, 2014, 49 (05) :2180-2186

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