Synthesis and X-ray crystal structure of a novel neutral trinuclear copper(II) hydridotris(3,5-dimethylpyrazolyl)borate complex with 1,1-azido bridges

被引:38
作者
Lam, MHW
Tang, YY
Fung, KM
You, XZ
Wong, WT
机构
[1] NANJING UNIV,INST COORDINAT CHEM,NANJING 210008,PEOPLES R CHINA
[2] UNIV HONG KONG,DEPT CHEM,HONG KONG,HONG KONG
关键词
D O I
10.1039/a700666g
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The X-ray crystal structure and magnetic properties of a neutral trinuclear 1,1-azido bridged copper(II) complex [LCu(mu-N-3)(2)Cu(mu-N-3)(2)CuL] 2 [L = hydridotris(3,5-dimethylpyrazolyl)borate], produced from the reaction between [Cu3L2]Cl 1 and an excess of trimethylsilyl azide, are reported.
引用
收藏
页码:957 / 958
页数:2
相关论文
共 22 条
[1]  
ALLEN JO, 1970, J AM CHEM SOC, V92, P4475
[2]   MOLECULAR-STRUCTURE OF BIS[(HYDRIDOTRIS(1-PYRAZOLYL)BORATO)COPPER(I)] AND IMPLICATIONS FOR CERTAIN COPPER-CONTAINING PROTEINS [J].
ARCUS, CS ;
WILKINSON, JL ;
MEALLI, C ;
MARKS, TJ ;
IBERS, JA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1974, 96 (24) :7564-7565
[3]  
ARCUS CS, 1976, J AM CHEM SOC, V98, P711
[4]   CARBONYL CHEMISTRY OF GROUP IB METALS [J].
BRUCE, MI .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1972, 44 (02) :209-+
[5]   GROUP IB METAL CHEMISTRY .1. PREPARATION AND REACTIONS OF CARBONYL(HYDROTRIPYRAZOL-1-YLBORATO)COPPER(I) COMPLEX [J].
BRUCE, MI ;
OSTAZEWSKI, AP .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1973, (22) :2433-2436
[6]   DINUCLEAR COPPER(II) CRYPTATES OF MACROCYCLIC LIGANDS - SYNTHESIS, CRYSTAL-STRUCTURE, AND MAGNETIC-PROPERTIES - MECHANISM OF THE EXCHANGE INTERACTION THROUGH BRIDGING AZIDO LIGANDS [J].
COMARMOND, J ;
PLUMERE, P ;
LEHN, JM ;
AGNUS, Y ;
LOUIS, R ;
WEISS, R ;
KAHN, O ;
MORGENSTERNBADARAU, I .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1982, 104 (23) :6330-6340
[7]   SYNTHETIC STRATEGY, MAGNETIC AND SPECTROSCOPIC PROPERTIES OF THE TERPYRIDINE COMPLEXES [CU(TERPY)X(H2O)N]Y (X = NCO, NCS OR N3 - N = 0 OR 1 - Y = NO3 OR PF6) - CRYSTAL-STRUCTURES OF THE AZIDENITRATE AND AZIDENEXAFLUORO-PHOSPHATE [J].
CORTES, R ;
URTIAGA, MK ;
LEZAMA, L ;
LARRAMENDI, JIR ;
ARRIORTUA, MI ;
ROJO, T .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1993, (24) :3685-3694
[8]   CATALYTIC METHODS FOR METAL CARBENE TRANSFORMATIONS [J].
DOYLE, MP .
CHEMICAL REVIEWS, 1986, 86 (05) :919-939
[9]  
EVANS DA, 1911, J AM CHEM SOC, V113, P728
[10]   CRYSTAL-STRUCTURE AND MAGNETIC-PROPERTIES OF (MU-AZIDO) (MU-HYDROXO)BIS[(N,N,N',N'-TETRAMETHYLETHYLENEDIAMINE)COPPER(II)] PERCHLORATE, A COPPER(II) DINUCLEAR COMPLEX WITH A LARGE FERROMAGNETIC INTERACTION [J].
KAHN, O ;
SIKORAV, S ;
GOUTERON, J ;
JEANNIN, S ;
JEANNIN, Y .
INORGANIC CHEMISTRY, 1983, 22 (20) :2877-2883