Temperature, heat and heat flow rate calibration of differential scanning calorimeters

被引：56
作者：
Gmelin, E
Sarge, SM
机构：
[1] Max Planck Inst Festkorperforsch, D-70569 Stuttgart, Germany
[2] Phys Tech Bundesanstalt, D-38116 Braunschweig, Germany
来源：
THERMOCHIMICA ACTA | 2000年 / 347卷 / 1-2期
关键词：
differential scanning calorimeters; calibration of DSC; calibration of temperature; heat calibration; heat flow rate calibration;
D O I：
10.1016/S0040-6031(99)00424-4
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
This contribution discusses basic problems and fundamental requirements for a universally applicable, unified and metrologically correct calibration of differential scanning calorimeters (DSC). The essential features of previously published recommendations of the German Society for Thermal Analysis (GEFTA) [see Hohne et al., Thermochim. Acta 160 (1990) 112; Cammenga et al., Thermochim. Acta 219 (1993) 333-343; Sarge et al., Thermochim. Acta 247 (1994) 129-168; J. Thermal Anal. 49 (1997) 1125-1134] developed for a correct and instrument-independent calibration of temperature, heat and heat flow rate of DSC, are outlined. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：9 / 13
页数：5
相关论文
共 19 条
  • [1] DEVELOPMENT OF STANDARD OPERATING PROCEDURES FOR DIFFERENTIAL SCANNING CALORIMETERS
    CALLANAN, JE
    SULLIVAN, SA
    [J]. REVIEW OF SCIENTIFIC INSTRUMENTS, 1986, 57 (10) : 2584 - 2592
  • [2] THE TEMPERATURE CALIBRATION OF SCANNING CALORIMETERS .2. CALIBRATION SUBSTANCES
    CAMMENGA, HK
    EYSEL, W
    GMELIN, E
    HEMMINGER, W
    HOHNE, GWH
    SARGE, SM
    [J]. THERMOCHIMICA ACTA, 1993, 219 : 333 - 342
  • [3] *DIN, 1994, INT VOC BAS GEN TERM
  • [4] CALIBRATION OF DIFFERENTIAL SCANNING CALORIMETERS
    GMELIN, E
    SARGE, SM
    [J]. PURE AND APPLIED CHEMISTRY, 1995, 67 (11) : 1789 - 1800
  • [5] Haines PJ, 1998, HBK THERMAL ANAL CAL, V1, P279
  • [6] Hemminger W., 1984, Calorimetry-fundamentals and practice
  • [7] Hemminger W.F., 1989, Methoden Des Thermischen Analyse
  • [8] Hill J. O., 1991, BETTER THERMAL ANAL
  • [9] THE TEMPERATURE CALIBRATION OF SCANNING CALORIMETERS
    HOHNE, GWH
    CAMMENGA, HK
    EYSEL, W
    GMELIN, E
    HEMMINGER, W
    [J]. THERMOCHIMICA ACTA, 1990, 160 (01) : 1 - 12
  • [10] SOME PECULIARITIES OF THE DSC-2/DSC-7 (PERKIN-ELMER) AND THEIR INFLUENCE ON ACCURACY AND PRECISION OF THE MEASUREMENTS
    HOHNE, GWH
    GLOGGLER, E
    [J]. THERMOCHIMICA ACTA, 1989, 151 : 295 - 304
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