Chemiluminescent nitrogen detection for HPLC: An important new tool in organic analytical chemistry

被引：50

作者：

Fitch, WL ^{[1
]}

Szardenings, AK ^{[1
]}

Fujinari, EM ^{[1
]}

机构：

[1] ANTEK INSTRUMENTS,HOUSTON,TX 77090

来源：

TETRAHEDRON LETTERS | 1997年 / 38卷 / 10期

关键词：

D O I：

10.1016/S0040-4039(97)00191-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Chemiluminescent nitrogen detection for HPLC is an important new high throughput technique for measuring yields and purities in synthetic organic chemistry. This destructive detector measures the total nitrogen content of a chromatographic peak, can be calibrated with any nitrogen containing compound, and thus allows quantitative analysis when authentic reference standards are not available. The application to solid phase synthesis is illustrated with a diketopiperazine synthesis. (C) 1997 Elsevier Science Ltd.

引用

页码：1689 / 1692

页数：4

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