Novel convenient one-pot method for the synthesis of indoloquinolines

被引：5
|
作者：
Aksenov, N. A. [1 ]
Gasanova, A. Z. [1 ]
Abakarov, G. M. [2 ]
Aksenova, I., V [1 ]
Aksenov, A., V [1 ]
机构：
[1] North Caucasus Fed Univ, 1A Ul Pushkina, Stavropol 355009, Russia
[2] Dagestan State Tech Univ, 70 Ul Imama Shamilya, Makhachkala 367010, Russia
来源：
RUSSIAN CHEMICAL BULLETIN | 2019年 / 68卷 / 04期
基金：
俄罗斯科学基金会;
关键词：
Fischer indole synthesis; isocryptolepine; reduction; one-pot synthesis; indole; Cryptolepis Sanguinolenta; BIOLOGICAL-ACTIVITIES; ISOCRYPTOLEPINE; ALKALOIDS; CRYPTOLEPINE; CRYPTOSANGUINOLENTINE; CRYPTOTACKIEINE; ROUTE; DERIVATIVES;
D O I：
10.1007/s11172-019-2493-4
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A novel one-pot method based on the sequence of the Fisher reaction between nitroacetophenone and phenylhydrazines, the reduction with metallic tin directly in polyphosphoric acid, and acylation has been developed for the synthesis of indoloquinolines. The obtained indolo-[3,2-c]quinolines are precursors of the analogs of isocryptolepine alkaloid.
引用
收藏
页码：836 / 840
页数：5
相关论文
共 50 条
  • [21] A Convenient One-pot Synthesis of Chromenyl Acrylates and Acrylonitriles
    Lopes, Diogo
    Costa, Marta
    Loucano, Joao
    Proenca, Fernanda
    SYNLETT, 2020, 31 (13) : 1298 - 1302
  • [22] A convenient one-pot synthesis of cyclohexenic primary amines
    Barbot, F
    Aidene, M
    Miginiac, L
    SYNTHETIC COMMUNICATIONS, 1998, 28 (17) : 3279 - 3289
  • [23] CONVENIENT ONE-POT SYNTHESIS OF DL-PYROCIN
    SCOTT, F
    NKWELO, MM
    SYNTHETIC COMMUNICATIONS, 1985, 15 (12) : 1051 - 1056
  • [24] A convenient one-pot synthesis of 6-trifluoromethylpyridines
    Katsuyama, I
    Ogawa, S
    Nakamura, H
    Yamaguchi, Y
    Funabiki, K
    Matsui, M
    Muramatsu, H
    Shibata, K
    HETEROCYCLES, 1998, 48 (04) : 779 - 785
  • [25] A one-pot and convenient synthesis of coumarins in solventless system
    Shockravi, A
    Valizadeh, H
    Heravi, MM
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2003, 178 (03) : 501 - 504
  • [26] Efficient and convenient one-pot synthesis of phosphoramidates and phosphates
    Gupta, A. K.
    Acharya, J.
    Dubey, D. K.
    Kaushik, M. P.
    SYNTHETIC COMMUNICATIONS, 2007, 37 (19-21) : 3403 - 3407
  • [27] A convenient one-pot synthesis of cyclohexenic primary amines
    Lab. de Synthèse Organique, URA 574 CNRS, Université de Poitiers, 40, avenue du Recteur Pineau, 86022 Poitiers, France
    Synth. Commun., 17 (3279-3289):
  • [28] Convenient one-pot synthesis and structures of pentaphenyltellurium monohalides
    Minoura, M
    Sagami, T
    Akiba, K
    ORGANOMETALLICS, 2001, 20 (12) : 2437 - 2439
  • [29] A CONVENIENT ONE-POT SYNTHESIS OF ALPHA-HALOACYLSILANES
    PAGE, PCB
    ROSENTHAL, S
    TETRAHEDRON LETTERS, 1986, 27 (44) : 5421 - 5422
  • [30] A CONVENIENT ONE-POT SYNTHESIS OF POLYENIC ENOL ETHERS
    VOQUANG, Y
    CARNIATO, D
    VOQUANG, L
    LEGOFFIC, F
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1983, (24) : 1505 - 1506
12345