Hydrothermal Synthesis and Characterization of Bi2MoO6 Nanoplates and Their Photocatalytic Activities

被引:28
|
作者
Phuruangrat, Anukorn [1 ]
Jitrou, Pimchanok [1 ]
Dumrongrojthanath, Phattharanit [2 ]
Ekthammathat, Nuengruethai [2 ]
Kuntalue, Budsabong [3 ]
Thongtem, Somchai [4 ,5 ]
Thongtem, Titipun [2 ,5 ]
机构
[1] Prince Songkla Univ, Fac Sci, Dept Mat Sci & Technol, Hat Yai 90112, Songkhla, Thailand
[2] Chiang Mai Univ, Fac Sci, Dept Chem, Chiang Mai 50200, Thailand
[3] Chiang Mai Univ, Fac Sci, Electron Microscopy Res & Serv Ctr, Chiang Mai 50200, Thailand
[4] Chiang Mai Univ, Fac Sci, Dept Phys & Mat Sci, Chiang Mai 50200, Thailand
[5] Chiang Mai Univ, Fac Sci, Mat Sci Res Ctr, Chiang Mai 50200, Thailand
关键词
VISIBLE-LIGHT; CONTROLLABLE SYNTHESIS; GAMMA-BI2MOO6; DEGRADATION; PERFORMANCE; MORPHOLOGY; NANOSHEETS;
D O I
10.1155/2013/789705
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The pH effect of the precursor solutions on the phase, morphologies, and photocatalytic activity of Bi2MoO6 synthesized by a hydrothermal reaction at 180 degrees C for 20 h was investigated. X-ray powder diffraction (XRD), Raman spectroscopy, Fourier transform infrared (FTIR) spectrometry, scanning electron microscopy (SEM), and transmission electron microscopy (TEM) revealed the presence of pure orthorhombic well-crystallized gamma-Bi2MoO6 nanoplates, including the symmetric (A(1g)) and asymmetric (A(2u)) stretching vibrations of the MoO6 octahedrons involving the motion of apical oxygen atoms. The photocatalytic activity of Bi2MoO6 nanoplates at the pH 6 determined via the decomposition of rhodamine-B (RhB) organic dye was the highest at 98.66% decolorization under Xe light irradiation.
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收藏
页数:8
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