Simultaneous determination of polyphenolic compounds in red and white grapes grown in Sardinia by high performance liquid chromatography-electron spray ionisation-mass spectrometry

被引：46

作者：

Hollecker, Laurent ^{[1
]}

Pinna, Maurizio ^{[1
]}

Filippino, Giorgia ^{[1
]}

Scrugli, Stefania ^{[1
]}

Pinna, Barbara ^{[2
]}

Argiolas, Francesca ^{[2
]}

Murru, Mariano ^{[2
]}

机构：

[1] Saras Ric & Tecnol Spa, I-09032 Assemini, CA, Italy

[2] Argiolas Spa, I-09040 Serdiana, CA, Italy

来源：

JOURNAL OF CHROMATOGRAPHY A | 2009年 / 1216卷 / 15期

关键词：

HPLC/ESI-MS/MS; Phenolic derivatives; Grape skins; Grape seeds; Screening; Flavonoid; Nonflavonoid; Fast-LC; VITIS-VINIFERA L; PHENOLIC-COMPOUNDS; HPLC ANALYSIS; WINES; EXTRACTION;

D O I：

10.1016/j.chroma.2009.02.010

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A new method for the identification and the quantification of nonanthocyanin phenolic compounds from six Vitis Vinifera grape varieties native to Sardinia (three native: Vermentino, Malvasia and Cannonau and three non-native types: Chardonnay, Sauvignon and Cabernet Sauvignon; Argiolas vineyard) was developed. This rapid and selective method employs LC/ESI-MS in negative mode. Different solvents extraction and different sorbents for purification were compared to the direct analysis of the initial extracts without further sample preparation. A total of 54 phenolic compounds were identified either in the freeze-dried skins or seeds, including nonflavonoids (hydroxybenzoic and hydroxycinnamic acids and their derivatives, stilbenes) and flavonoids (flavanols, flavonols, dihydroxyflavonols). (C) 2009 Elsevier B.V. All rights reserved.

引用

页码：3402 / 3408

页数：7

共 24 条

[1]

BOURZEIX M, 1986, B OIV, P669

[2] Analysis of phenolic compounds in Muscatel wines produced in Portugal [J].

Bravo, MN ;

Silva, S ;

Coelho, AV ;

Boas, LV ;

Bronze, MR .

ANALYTICA CHIMICA ACTA, 2006, 563 (1-2) :84-92

[3] Levels of flavan-3-ols in French wines [J].

Carando, S ;

Teissedre, PL ;

Pascual-Martinez, L ;

Cabanis, JC .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (10) :4161-4166

[4]

CRAVERO MC, 1996, ENOTECNICO MAR

[5]

Di Stefano R., 1991, Rivista di Viticoltura e di Enologia, V44, P37

[6]

DISTEFANO R, 2002, ENOLOGO OCT, P82

[7]

DISTEFANO R, 1995, ENOTECNICO, V29, P75

[8] Solid-phase extraction for sample preparation, in the HPLC analysis of polyphenolic compounds in ''fino'' sherry wine [J].

Guillen, DA ;

Merello, F ;

Barroso, CG ;

PerezBustamante, JA .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (02) :403-406

[9]

Ibern-Gómez M, 2002, AM J ENOL VITICULT, V53, P218

[10]

Jordao AM, 2001, AM J ENOL VITICULT, V52, P230

← 1 2 3 →