New dynamic diamond anvil cells for tera-pascal per second fast compression x-ray diffraction experiments

被引:41
|
作者
Jenei, Zs. [1 ]
Liermann, H. P. [2 ]
Husband, R. [2 ]
Mendez, A. S. J. [2 ]
Pennicard, D. [2 ]
Marquardt, H. [3 ]
O'Bannon, E. F. [1 ]
Pakhomova, A. [2 ]
Konopkova, Z. [2 ,4 ]
Glazyrin, K. [1 ]
Wendt, M. [2 ]
Wenz, S. [2 ]
McBride, E. E. [2 ,7 ]
Morgenroth, W. [5 ]
Winkler, B. [5 ]
Rothkirch, A. [2 ]
Hanfland, M. [6 ]
Evans, W. J. [1 ]
机构
[1] Lawrence Livermore Natl Lab, High Pressure Phys Grp, 7000 East Ave,L-041, Livermore, CA 94550 USA
[2] DESY, Photon Sci, Notkestr 85, D-22607 Hamburg, Germany
[3] Univ Oxford, Dept Earth Sci, South Parks Poad, Oxford OX1 3AN, England
[4] European Xray Free Electron Laser Facil GmbH, Holzkoppel 4, D-22869 Schenefeld, Germany
[5] Goethe Univ Frankfurt, Dept Geosci, Arbeitsgrp Kristallog, D-60438 Frankfurt, Germany
[6] ESPF, European Synchrotron, 71 Ave Martyrs, F-38000 Grenoble, France
[7] SLAC Natl Accelerator Lab, 2575 Sand Hill Pd, Menlo Pk, CA 94025 USA
关键词
EQUATION-OF-STATE; D2O ICE VII; HIGH-PRESSURE; POWDER DIFFRACTION; PHASE-TRANSITIONS; ALPHA-QUARTZ;
D O I
10.1063/1.5098993
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Fast compression experiments performed using dynamic diamond anvil cells (dDACs) employing piezoactuators offer the opportunity to study compression-rate dependent phenomena. In this paper, we describe an experimental setup which allows us to perform time-resolved x-ray diffraction during the fast compression of materials using improved dDACs. The combination of the high flux available using a 25.6 keV x-ray beam focused with a linear array of compound refractive lenses and the two fast GaAs LAMBDA detectors available at the Extreme Conditions Beamline (P02.2) at PETRA III enables the collection of x-ray diffraction patterns at an effective repetition rate of up to 4 kHz. Compression rates of up to 160 TPa/s have been achieved during the compression of gold in a 2.5 ms fast compression using improved dDAC configurations with more powerful piezoactuators. The application of this setup to low-Z compounds at lower compression rates is described, and the high temporal resolution of the setup is demonstrated. The possibility of applying finely tuned pressure profiles opens opportunities for future research, such as using oscillations of the piezoactuator to mimic propagation of seismic waves in the Earth.
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页数:12
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