Effect of pyrolyzation temperature on wood-derived carbon and silicon carbide

被引:37
作者
Pappacena, K. E. [1 ]
Gentry, S. P. [1 ]
Wilkes, T. E. [1 ]
Johnson, M. T. [1 ]
Xie, S. [1 ]
Davis, A. [1 ]
Faber, K. T. [1 ]
机构
[1] Northwestern Univ, Dept Mat Sci & Engn, Evanston, IL 60208 USA
基金
美国国家科学基金会;
关键词
Porosity; Carbon; SiC; Spectroscopy; X-ray methods; MECHANICAL-PROPERTIES; CERAMICS; GRAPHITIZATION; MICROSTRUCTURE;
D O I
10.1016/j.jeurceramsoc.2009.04.040
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The structure of carbon and silicon carbide produced through the pyrolyzation of wood and the subsequent melt-infiltration with silicon was studied as a function of initial carbon pyrolyzation temperature. Scanning electron microscopy, transmission electron microscopy, mercury intrusion porosimetry, X-ray diffraction and Raman spectroscopy were used to characterize material derived from initial carbon pyrolyzation temperatures in the range of 300-2400 degrees C. It was determined that, although structural differences abound in carbon pyrolyzed at different temperatures, the resulting silicon carbide is independent of the initial temperature of carbon pyrolyzation. (C) 2009 Elsevier Ltd. All rights reserved.
引用
收藏
页码:3069 / 3077
页数:9
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