An Efficient Synthesis of 14-Aryl or Alkyl-14H-dibenzo[a.j]xanthenes Using Reusable HBF4-SiO2 Catalyst Under Thermal and Solvent-Free Conditions

被引：9

作者：

Fu, Gui-Yun ^{[1
]}

Huang, Yi-Xiang ^{[1
]}

Chen, Xiao-Gang ^{[1
]}

Liu, Xiao-Ling ^{[1
]}

机构：

[1] Jiangxi Normal Univ, Coll Chem & Chem Engn, Nanchang 330022, Peoples R China

来源：

JOURNAL OF THE CHINESE CHEMICAL SOCIETY | 2009年 / 56卷 / 02期

关键词：

Xanthene; HBF4-SiO2; Aldehyde; beta-Naphthol; Solvent-free; One-pot condensation; LEUCO-DYE DERIVATIVES; ONE-POT SYNTHESIS; HETEROGENEOUS CATALYST; MICROWAVE IRRADIATION; DIBENZOXANTHENES; ALCOHOLS; SILICA; ACID; ARYL;

D O I：

10.1002/jccs.200900055

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A simple and convenient procedure for the synthesis of 14-aryl or alkyl-14H-dibenzo[a.j]xanthene derivatives is described through a one-pot condensation of beta-naphthol with various aryl or alkyl aldehydes in the presence of HBF4-SiO2 as the catalyst under thermal and solvent-free conditions.

引用

页码：381 / 385

页数：5

共 28 条

[1] Heteropolyacid:: An efficient and eco-friendly catalyst for the synthesis of 14-aryl-14H-dibenzo[a,j]xanthene
Amini, Mostafa Mohammadpour
Seyyedhamzeh, Mozhdeh
Bazgir, Ayoob
[J]. APPLIED CATALYSIS A-GENERAL, 2007, 323 : 242 - 245
[2] CHEMICAL ASPECTS OF SANTALIN AS A HISTOLOGICAL STAIN
BANERJEE, A
MUKHERJEE, AK
[J]. STAIN TECHNOLOGY, 1981, 56 (02): : 83 - 85
[3] Fluoroboric acid adsorbed on silica gel as a new and efficient catalyst for acylation of phenols, thiols, alcohols, and amines
Chakraborti, AK
Gulhane, R
[J]. TETRAHEDRON LETTERS, 2003, 44 (17) : 3521 - 3525
[4] Iodine catalyzed simple and efficient synthesis of 14-aryl or alkyl-14-H-dibenzo[a,j]xanthenes
Das, Biswanath
Ravikanth, B.
Ramu, R.
Laxminarayana, K.
Rao, B. Vittal
[J]. JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2006, 255 (1-2) : 74 - 77
[5] Hideo T., 1981, Patent Japan, Patent No. [56005480, JP56005480]
[6] The incorporation of various porphyrins into blood cells measured via flow cytometry, absorption and emission spectroscopy
Ion, RM
Planner, A
Wiktorowicz, K
Frackowiak, D
[J]. ACTA BIOCHIMICA POLONICA, 1998, 45 (03) : 833 - 845
[7] KHORAMABADIZAD A, 2002, J KOREAN CHEM SOC, V46, P541
[8] KHORRAMABADIZAD A, 2007, J CHEM RES S, P277
[9] A facile, simple and convenient method for the synthesis of 14-alkyl or aryl-14-H-dibenzo[a,j]xanthenes catalyzed by pTSA in solution and solvent-free conditions
Khosropour, AR
Khodaei, MM
Moghannian, H
[J]. SYNLETT, 2005, (06) : 955 - 958
[10] XANTHENE-DYE-LABELED PHOSPHATIDYLETHANOLAMINES AS PROBES OF INTERFACIAL PH - STUDIES IN PHOSPHOLIPID-VESICLES
KNIGHT, CG
STEPHENS, T
[J]. BIOCHEMICAL JOURNAL, 1989, 258 (03) : 683 - 687

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