Characterization of Bi2S3 nanorods and nano-structured flowers prepared by a hydrothermal method

被引：51
作者：
Phuruangrat, Anukorn [1 ]
Thongtem, Titipun [2 ]
Thongtem, Somchai [1 ]
机构：
[1] Chiang Mai Univ, Dept Phys & Mat Sci, Fac Sci, Chiang Mai 50200, Thailand
[2] Chiang Mai Univ, Dept Chem, Fac Sci, Chiang Mai 50200, Thailand
来源：
MATERIALS LETTERS | 2009年 / 63卷 / 17期
关键词：
Bismuth sulfide; Nanorods; Nano-structured flowers; Hydrothermal method; OPTICAL-PROPERTIES; FACILE SYNTHESIS; US NANOWIRES; MORPHOLOGIES;
D O I：
10.1016/j.matlet.2009.03.051
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Bismuth sulfide nanorods and nano-structured flowers were synthesized by hydrothermal reaction of bismuth nitrate pentahydrate and thiourea solutions, containing 1 and 2 ml of 65% HNO3. respectively. By using X-ray diffraction (XRD), selected area electron diffraction (SAED), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and high resolution TEM (HRTEM), the products were specified as orthorhombic Bi2S3 in the shapes of nanorods and flower-like clusters of nanorods, with the growth of nanorods in the [001] direction. A diffraction pattern was also simulated, and was in good accordance with the SAED pattern obtained from the experiment. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码：1496 / 1498
页数：3
相关论文
共 14 条
  • [1] Boudias C., 1989, CARINE CRYSTALLOGRAP
  • [2] A very simple and low cost route to Bi2S3 nanorods bundles and dandelion-like nanostructures
    Dong, Lihong
    Chu, Ying
    Zhang, Wei
    [J]. MATERIALS LETTERS, 2008, 62 (27) : 4269 - 4272
  • [3] Preparation of Bi2S3 nanowhiskers and their morphologies
    He, R
    Qian, XF
    Yin, J
    Zhu, ZK
    [J]. JOURNAL OF CRYSTAL GROWTH, 2003, 252 (04) : 505 - 510
  • [4] JCPDS-International Centre for Diffraction Data, 2001, POWD DIFFR FIL, P19073
  • [5] Synthesis and growth mechanism of Bi2S3 nanoribbons
    Liu, ZP
    Liang, JB
    Li, S
    Peng, S
    Qian, Y
    [J]. CHEMISTRY-A EUROPEAN JOURNAL, 2004, 10 (03) : 634 - 640
  • [6] Microwave-assisted synthesis and characterization of 3D flower-like Bi2S3 superstructures
    Lu, Juan
    Han, Qiaofeng
    Yang, Xujie
    Lu, Lude
    Wang, Xin
    [J]. MATERIALS LETTERS, 2007, 61 (14-15) : 2883 - 2886
  • [7] Preparation of Bi2S3 nanorods via a hydrothennal approach
    Lu, Juan
    Han, Qiaofeng
    Yang, Xujie
    Lu, Lude
    Wang, Xin
    [J]. MATERIALS LETTERS, 2007, 61 (16) : 3425 - 3428
  • [8] Optical properties of US nanowires prepared by dc electrochemical deposition in porous alumina template
    Mondal, S. P.
    Dhar, A.
    Ray, S. K.
    [J]. MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 2007, 10 (4-5) : 185 - 193
  • [9] Facile synthesis and characterization of single crystalline Bi2S3 with various morphologies
    Quan, Zewei
    Yang, Jun
    Yang, Piaoping
    Wang, Zhenling
    Li, Chunxia
    Lin, Jun
    [J]. CRYSTAL GROWTH & DESIGN, 2008, 8 (01) : 200 - 207
  • [10] The effect of agitation states on hydrothermal synthesis of Bi2S3 nanorods
    Shao, MW
    Mo, MS
    Cui, Y
    Chen, G
    Qian, YT
    [J]. JOURNAL OF CRYSTAL GROWTH, 2001, 233 (04) : 799 - 802
12