X-ray powder diffraction in reflection geometry on multi-beam kJ-type laser facilities

被引:10
作者
Denoeud, A. [1 ]
Hernandez, J-A [2 ,3 ]
Vinci, T. [2 ]
Benuzzi-Mounaix, A. [2 ]
Brygoo, S. [1 ]
Berlioux, A. [2 ]
Lefevre, F. [2 ]
Sollier, A. [1 ,4 ]
Videau, L. [1 ,4 ]
Ravasio, A. [2 ]
Guarguaglini, M. [2 ]
Duthoit, L. [1 ]
Loison, D. [5 ]
Brambrink, E. [2 ,6 ]
机构
[1] CEA, DAM, DIF, F-91297 Arpajon, France
[2] Sorbonne Univ, Inst Polytech Paris, Ecole Polytech, CEA,CNRS,LULI, F-91128 Palaiseau, France
[3] Univ Oslo, Ctr Earth Evolut & Dynam, Box 1028 Blindern, N-0315 Oslo, Norway
[4] Univ Paris Saclay, Lab Matiere Condit Extremes, CEA, F-91680 Bruyeres Le Chatel, France
[5] Univ Rennes, IPR Inst Phys Rennes UMR 6251, CNRS, F-35000 Rennes, France
[6] European XFEL, Holzkoppel 4, D-22869 Schenefeld, Germany
关键词
SHOCK COMPRESSION; TRANSITION; IRON;
D O I
10.1063/5.0020261
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An ultrafast x-ray powder diffraction setup for laser-driven dynamic compression has been developed at the LULI2000 laser facility. X-ray diffraction is performed in reflection geometry from a quasi-monochromatic laser-generated plasma x-ray source. In comparison to a transmission geometry setup, this configuration allows us to probe only a small portion of the compressed sample, as well as to shield the detectors against the x-rays generated by the laser-plasma interaction on the front side of the target. Thus, this new platform facilitates probing of spatially and temporarily uniform thermodynamic conditions and enables us to study samples of a large range of atomic numbers, thicknesses, and compression dynamics. As a proof-of-concept, we report direct structural measurements of the bcc-hcp transition both in shock and ramp-compressed polycrystalline iron with diffraction signals recorded between 2 theta similar to 30 degrees and similar to 150 degrees. In parallel, the pressure and temperature history of probed samples is measured by rear-side visible diagnostics (velocimetry and pyrometry).
引用
收藏
页数:17
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