Single-Laboratory Validation Study of Determination of Patulin by GC-MS in Juice

被引：0

作者：

Hattori, Satoshi ^{[1
]}

Tsukada, Masanori ^{[1
]}

Morita, Mifumi ^{[2
]}

Suenaga, Kazuya ^{[2
]}

机构：

[1] Kobe Reg Ctr, Food & Agr Mat Inspect Ctr, Chuo Ku, 1-3-7 Minatojimaminamimachi, Kobe, Hyogo 6510082, Japan

[2] Headquarters Saitama Shintoshin Natl Govt Bldg Ke, Food & Agr Mat Inspect Ctr, Chuo Ku, 2-1 Shintoshin, Saitama 3309731, Japan

来源：

FOOD HYGIENE AND SAFETY SCIENCE | 2018年 / 59卷 / 03期

关键词：

GC-MS; validation study; apple juice; pear juice; patulin; MASS-SPECTROMETRY; APPLE JUICE; CONFIRMATION; MYCOTOXINS;

D O I：

10.3358/shokueishi.59.157

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

We examined whether the analytical method of patulin (a mycotoxin found in fruit juice) developed in Nagano prefecture meets the criteria in the Codex Procedural Manual and Guidelines on Analytical Terminology. The trueness, repeatability, within-laboratory reproducibility and Hor-Rat value were 98.8-103.4%, less than 6.4, 8.1 and 0.4%, respectively, for apple juice and pear juice. Thus, the trueness and precision met the required criteria.

引用

页码：157 / 160

页数：4

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