Synthesis and characterization of conductive poly(o-anisidine)/talc composite

被引：3
|
作者：
Anakli, Duygu [1 ]
Cetinkaya, Sevil [1 ]
Karakisla, Meral [2 ]
Sacak, Ehmet [2 ]
机构：
[1] Cumhuriyet Univ, Muhendisl Fac, Kimya Muhendisligi Bolumu, TR-58140 Sivas, Turkey
[2] Ankara Univ, Fen Fak, Kimya Bolumu, TR-06100 Ankara, Turkey
来源：
JOURNAL OF THE FACULTY OF ENGINEERING AND ARCHITECTURE OF GAZI UNIVERSITY | 2018年 / 33卷 / 02期
关键词：
Poly (o-anisidine); talc; composite; conductive polymer; IN-SITU POLYMERIZATION; POLYANILINE/MONTMORILLONITE NANOCOMPOSITES; OXIDATIVE POLYMERIZATION; ELECTRICAL-PROPERTIES; ORGANIC COATINGS; SULFONIC-ACIDS; TALC; PERFORMANCE; POLYANILINE; PARTICLES;
D O I：
10.17341/gazimmfd.416349
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Conductive poly(o-anisidine) (POA)/talc composite was prepared by chemical polymerization of o-anisidine in the presence of talc using ammonium persulfate (APS) as oxidant. The polymerization parameters such as APS/o-anisidine mol ratio, o-anisidine and HCl concentration on the conductivity and POA amount of the POA/talc composite were investigated. The increased microhardness property of the talc particles by the addition of the conducting polymer was examined by micro indentation analysis. The structural, morphological and thermal properties of the composites were analyzed by using FTIR (Fourier transform infrared spectroscopy), XRD (X-ray diffraction), SEM (Scanning electron microscopy), BET (Brunauer-Emmett-Teller) surface area analysis and TGA (Thermogravimetric analysis) techniques.
引用
收藏
页码：403 / 412
页数：10
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