AN EFFICIENT ONE-POT SYNTHESIS OF NEW 2-THIOXO AND 2-OXO-PYRIMIDINE-5-CARBONITRILES IN BALL-MILLING UNDER SOLVENT-FREE AND CATALYST-FREE CONDITIONS

被引：12

作者：

M'hamed, Mohamed Ould ^{[1
]}

Alduaij, Omar K. ^{[1
]}

机构：

[1] Al Imam Mohammad Ibn Saud Islamic Univ IMSIU, Dept Chem, Coll Sci, Riyadh 11623, Saudi Arabia

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2014年 / 189卷 / 02期

关键词：

Ball milling solvent-free reaction; catalyst-free; thioxo-pyrimidine; oxo-pyrimidine; SOLID-STATE; WASTE-FREE; MECHANOCHEMISTRY; PYRIMIDINE;

D O I：

10.1080/10426507.2013.818995

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Various 2-thioxo and 2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carbonitriles were synthesized in very high yields in 40min through a direct condensation of an equimolar amount of an aldehyde, malononitrile, and thiourea/urea under ball mill solvent-free and catalyst-free conditions.

引用

收藏

页码：235 / 241

页数：7

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