Valorization of Citrus limon residues for the recovery of antioxidants: Evaluation and optimization of microwave and ultrasound application to solvent extraction

被引：147

作者：

Dahmoune, Farid ^{[1
]}

Boulekbache, Lila ^{[1
]}

Moussi, Kamal ^{[1
]}

Aoun, Omar ^{[1
]}

Spigno, Giorgia ^{[2
]}

Madani, Khodir ^{[1
]}

机构：

[1] Abderrahmane Mira Univ Bejaia, Lab Biomath Biochem Biophys & Scientometr, Bejaia 06000, Algeria

[2] Univ Cattolica Sacro Cuore, Inst Oenol & Food Engn, I-29122 Piacenza, Italy

来源：

INDUSTRIAL CROPS AND PRODUCTS | 2013年 / 50卷

关键词：

Citrus limon peels; Optimization; Microwave assisted extraction; Ultrasound assisted extraction; Phenolic compounds; ASSISTED EXTRACTION; PHENOLIC-COMPOUNDS; SEPARATION; LEAVES; ACIDS; L;

D O I：

10.1016/j.indcrop.2013.07.013

中图分类号：

S2 [农业工程];

学科分类号：

0828 ;

摘要：

Ultrasound assisted extraction (UAE) and microwave-assisted extraction (MAE) were optimized (by response surface methodology, RSM) and compared for the recovery of total phenolic compounds (TPC expressed as gallic acid equivalents (GAE)) from Citrus limon peels. The optimized result for MAE was 48% ethanol as extraction solvent, 28:1 mL/g of solvent: solid ratio, 123 s and 400 W for irradiation time and power. The optimized result for UAE was 63.93% ethanol as extraction solvent, 40 mL/g of liquid/solid ratio, 15.05 min of holding time and 77.79% for amplitude. Maximum predicted TPC recoveries under the optimized conditions for MAE and UAE were 15.74 and 15.08 mg GAE/g respectively, which were close to the experimental values of 15.78 +/- 0.8 and 15.22 +/- 0.88 mg GAE/g, indicating suitability of the employed model and the success of RSM in optimizing the extraction conditions. The antioxidant activity determined by the DPPH and reducing power tests confirmed the suitability of MAE for the preparation of antioxidant-rich plant extracts. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：77 / 87

页数：11

共 48 条

[1]

[Anonymous], 2002, CITRUS GENUS CITRUS

[2] Quality retention and potential shelf-life of fresh-cut lemons as affected by cut type and temperature [J].

Artes-Hernandez, Francisco ;

Rivera-Cabrera, Fernando ;

Kader, Adel A. .

POSTHARVEST BIOLOGY AND TECHNOLOGY, 2007, 43 (02) :245-254

[3] The effect of different extraction techniques on extraction yield, total phenolic, and anti-radical capacity of extracts from Pinus radiata Bark [J].

Aspe, Estrella ;

Fernandez, Katherina .

INDUSTRIAL CROPS AND PRODUCTS, 2011, 34 (01) :838-844

[4] Optimization of ultrasonic-assisted extraction of antioxidant compounds from blackberry leaves using response surface methodology [J].

Aybastier, Onder ;

Isik, Esra ;

Sahin, Saliha ;

Demir, Cevdet .

INDUSTRIAL CROPS AND PRODUCTS, 2013, 44 :558-565

[5] Ultrasound assisted extraction of phenolic compounds from grapes [J].

Carrera, Ceferino ;

Ruiz-Rodriguez, Ana ;

Palma, Miguel ;

Barroso, Carmelo G. .

ANALYTICA CHIMICA ACTA, 2012, 732 :100-104

[6] Comparative Study of Antioxidant Properties and Total Phenolic Content of 30 Plant Extracts of Industrial Interest Using DPPH, ABTS, FRAP, SOD, and ORAC Assays [J].

Dudonne, Stephanie ;

Vitrac, Xavier ;

Coutiere, Philippe ;

Woillez, Marion ;

Merillon, Jean-Michel .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2009, 57 (05) :1768-1774

[7]

Eskilsson CS, 2000, J CHROMATOGR A, V902, P227

[8] The effect of microwave assisted extraction on the isolation of anthocyanins and phenolic acids from sour cherry Marasca (Prunus cerasus var. Marasca) [J].

Garofulic, Ivona Elez ;

Dragovic-Uzelac, Verica ;

Jambrak, Anet Rezek ;

Jukic, Marijana .

JOURNAL OF FOOD ENGINEERING, 2013, 117 (04) :437-442

[9] Natural bioactive compounds of Citrus limon for food and health [J].

Gonzalez-Molina, E. ;

Dominguez-Perles, R. ;

Moreno, D. A. ;

Garcia-Viguera, C. .

JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2010, 51 (02) :327-345

[10] Microwave-assisted extraction and determination of cyanuric acid residue in infant formula samples by liquid chromatography-tandem mass spectrometry [J].

Han, Chao ;

Liu, Cuiping ;

Zhou, Yongfang ;

Xia, Biqi ;

Zhu, Zhenou ;

Lei, Xinxiang ;

Shen, Yan .

FOOD CHEMISTRY, 2011, 127 (02) :875-879

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