Hexakis(dimethyl sulfoxide)manganese(II) bis(perchlorate)

被引:12
作者
Migdal-Mikuli, A.
Szostak, E.
Nitek, W.
机构
[1] Jagiellonian Univ, Fac Chem, Dept Phys Chem, PL-30060 Krakow, Poland
[2] Jagiellonian Univ, Fac Chem, Dept Crystal Chem & Crystal Phys, PL-30060 Krakow, Poland
关键词
D O I
10.1107/S1600536806036026
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, [Mn(C2H6OS)(6)](ClO4)(2), comprises discrete [Mn(DMSO)(6)](2+) cations (DMSO is dimethyl sulfoxide) and perchlorate anions, all of which lie on crystallographic twofold axes. The O atoms of six DMSO molecules are bonded to the Mn-II ion in a distorted octahedral geometry.
引用
收藏
页码:M2581 / M2582
页数:2
相关论文
共 10 条
[1]   COMPLETION AND REFINEMENT OF CRYSTAL-STRUCTURES WITH SIR92 [J].
ALTOMARE, A ;
CASCARANO, G ;
GIACOVAZZO, C ;
GUAGLIARDI, A .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1993, 26 (pt 3) :343-350
[3]  
Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI DOI 10.1107/S0021889899006020
[4]   ON ENANTIOMORPH-POLARITY ESTIMATION [J].
FLACK, HD .
ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV) :876-881
[5]  
LUBEZNOWA TU, 1989, KRISTALLOGRAFIYA, V43, P862
[6]   Phase polymorphism of [Mn(DMSO)6](ClO4)2 studied by differential scanning calorimetry [J].
Migdal-Mikuli, A ;
Szostak, E .
ZEITSCHRIFT FUR NATURFORSCHUNG SECTION A-A JOURNAL OF PHYSICAL SCIENCES, 2005, 60 (04) :289-295
[7]  
Nonius, 1998, COLLECT
[8]   Processing of X-ray diffraction data collected in oscillation mode [J].
Otwinowski, Z ;
Minor, W .
MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 :307-326
[9]   CRYSTAL AND MOLECULAR-STRUCTURE OF HEXAKIS(DIMETHYL SULFOXIDE)CADMIUM(II) PERCHLORATE, [CD((CH3)2SO)6](CLO4)2 [J].
SANDSTROM, M .
ACTA CHEMICA SCANDINAVICA SERIES A-PHYSICAL AND INORGANIC CHEMISTRY, 1978, 32 (06) :519-525
[10]  
Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR