Development of a slurry injection technique for continuous fibre ultra-high temperature ceramic matrix composites

被引:40
作者
Baker, B. [1 ]
Rubio, V. [2 ]
Ramanujam, P. [3 ]
Binner, J. [1 ]
Hussain, A. [4 ]
Ackerman, T. [4 ]
Brown, P. [5 ]
Dautremont, I. [6 ]
机构
[1] Univ Birmingham, Sch Met & Mat, Birmingham, W Midlands, England
[2] Natl Composites Ctr, Bristol, Avon, England
[3] Wendt India Ltd, Hosur, India
[4] MBDA Missile Syst, Stevenage, Herts, England
[5] DSTL, Porton Down, England
[6] DGA, Paris, France
基金
英国工程与自然科学研究理事会;
关键词
Ceramic matrix composites; Slurry impregnation; CT analysis; Injection; Ultra-high temperature ceramics; C-F/SIC COMPOSITES; ABLATION PROPERTIES; SIC COMPOSITES; MICROSTRUCTURE; INFILTRATION; FABRICATION; DESIGN; POWDER;
D O I
10.1016/j.jeurceramsoc.2019.05.070
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
A simple and effective slurry injection method for producing dense and uniform ultra-high ceramic matrix composites from preforms of high fibre density was developed. As this method is based on slurry injection the homogeneity is not constrained to small preform sizes; dense components of high fibre volume can be produced in theoretically any size and shape. Samples produced by this method demonstrated high and consistent densities, with the injection method obtaining densities an average 27% higher and 87% lower in variability when compared to conventional vacuum impregnation. Tomography demonstrated no bias in the ceramic powder distribution for samples produced by injection, whereas samples produced by vacuum impregnation alone displayed poor powder penetration to the centre of large samples. The new approach yielded composites that were as strong and/or more consistent in strength compared to vacuum impregnation. Thermo-ablative testing demonstrated significant improvements in protective capability for materials produced by this route.
引用
收藏
页码:3927 / 3937
页数:11
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