3-[3-(Trifluoromethyl)anilino]isobenzofuran-1(3H)-one

被引：7
作者：
Odabasoglu, Mustafa [1 ]
Buyukgungor, Orhan
机构：
[1] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Chem, TR-55139 Kurupelit, Turkey
[2] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Kurupelit, Turkey
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷
关键词：
D O I：
10.1107/S1600536806032089
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Crystals of the title compound, C15H10F3NO3, are stabilized by N - (HO)-O-... and C - (HO)-O-... intermolecular hydrogen bonds and by weak C - H-...pi interactions. In the structure, paired C (HO)-O-... hydrogen bonds link the molecules into R-2(2)( 10) dimers. The hydrogen-bonded R-2(2)(10) dimers are linked by intermolecular N - (HO)-O-... hydrogen bonds and generate R-6(4)(22) rings. The phthalide section of the molecule is planar and the dihedral angle between the phthalide group and the benzene ring is 56.31 ( 17)degrees.
引用
收藏
页码：O4151 / O4153
页数：3
相关论文
共 10 条
[1]   ENCODING AND DECODING HYDROGEN-BOND PATTERNS OF ORGANIC-COMPOUNDS [J].
ETTER, MC .
ACCOUNTS OF CHEMICAL RESEARCH, 1990, 23 (04) :120-126
[2]   ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI) [J].
Journal of Applied Crystallography, 1997, 30 (pt 5)
[3]  
Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI DOI 10.1107/S0021889899006020
[4]   3-(4-hydroxyanilino)isobenzofuran-1 (3H)-one [J].
Odabasoglu, M ;
Büyükgüngör, O .
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 :O1879-O1881
[5]   3-[2-(trifluoromethyl)anilino]isobenzofuran-1(3H)-one [J].
Odabasoglu, Mustafa ;
Buyukgungor, Orhan .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O4148-O4150
[6]   3-(4-Acetylanilino)isobenzofuran-1(3H)-one [J].
Odabasoglu, Mustafa ;
Buyukgungor, Orhan .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O4145-O4147
[7]   3-Anilinoisobenzofuran-1(3H)-one [J].
Odabasoglu, Mustafa ;
Buyukgungor, Orhan .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :O2943-O2944
[8]  
Sheldrick G. M., 1997, SHELXL97
[9]   PHASE ANNEALING IN SHELX-90 - DIRECT METHODS FOR LARGER STRUCTURES [J].
SHELDRICK, GM .
ACTA CRYSTALLOGRAPHICA SECTION A, 1990, 46 :467-473
[10]  
Stoe & Cie, 2002, X AREA VERS 1 18 X R
1